(2R,6S,7R,9R,14S)-14-tert-Butyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

Base Information

Chemical Name:(2R,6S,7R,9R,14S)-14-tert-Butyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane
CAS No.:156599-71-2
Molecular Formula:C₂₈H₃₆O₄
Molecular Weight:436.591
Hs Code.:

Synonyms:(2R,6S,7R,9R,14S)-14-tert-Butyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

Suppliers and Price of (2R,6S,7R,9R,14S)-14-tert-Butyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,6S,7R,9R,14S)-14-tert-Butyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (2R,6S,7R,9R,14S)-14-tert-Butyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

There total 3 articles about (2R,6S,7R,9R,14S)-14-tert-Butyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 59562-82-2
3,3-dimetylbutan-1,2-diol

: 156599-77-8
(2R,6S,7R,9R,14S)-14-Benzyloxymethyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

: 156599-71-2
(2R,6S,7R,9R,14S)-14-tert-Butyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

Guidance literature:: With camphor-10-sulfonic acid; In toluene; at 110 ℃;
DOI:10.1016/0957-4166(94)80016-2

Reference yield: 90.0%

: 59562-82-2
3,3-dimetylbutan-1,2-diol

: 154859-08-2
<2R,2'R> 2,2-diphenyl-3,3',4,4'-tetrahydro-6,6'-bi-2H-pyran

: 156599-71-2
(2R,6S,7R,9R,14S)-14-tert-Butyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

Guidance literature:: With camphor-10-sulfonic acid; In toluene; at 110 ℃; for 48h;
DOI:10.1016/0957-4166(94)80016-2

Reference yield:

: 6920-22-5
Hexane-1,2-diol

: 156599-77-8
(2R,6S,7R,9R,14S)-14-Benzyloxymethyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

: 56552-80-8
(R)-3-benzyloxy-1,2-propanediol

: 156599-71-2
(2R,6S,7R,9R,14S)-14-tert-Butyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

Guidance literature:: With camphor-10-sulfonic acid; In toluene; at 110 ℃; Yield given. Yields of byproduct given;
DOI:10.1016/0957-4166(94)80016-2