(2R,6S,7R,9R,14S)-14-Benzyloxymethyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

Base Information

Chemical Name:(2R,6S,7R,9R,14S)-14-Benzyloxymethyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane
CAS No.:156599-77-8
Molecular Formula:C₃₂H₃₆O₅
Molecular Weight:500.635
Hs Code.:

Synonyms:(2R,6S,7R,9R,14S)-14-Benzyloxymethyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,6S,7R,9R,14S)-14-Benzyloxymethyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

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Technology Process of (2R,6S,7R,9R,14S)-14-Benzyloxymethyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

There total 1 articles about (2R,6S,7R,9R,14S)-14-Benzyloxymethyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 56-81-5,25618-55-7,64333-26-2,8013-25-0
glycerol

: 156599-71-2
(2R,6S,7R,9R,14S)-14-tert-Butyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

: 156599-77-8
(2R,6S,7R,9R,14S)-14-Benzyloxymethyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

Guidance literature:: With camphor-10-sulfonic acid; sodium hydride; Yield given. Multistep reaction; 1.) PhMe, 110 deg C, 2.) THF;
DOI:10.1016/0957-4166(94)80016-2

Reference yield: 93.0%

: 59562-82-2
3,3-dimetylbutan-1,2-diol

: 156599-77-8
(2R,6S,7R,9R,14S)-14-Benzyloxymethyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

: 156599-71-2
(2R,6S,7R,9R,14S)-14-tert-Butyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

Guidance literature:: With camphor-10-sulfonic acid; In toluene; at 110 ℃;
DOI:10.1016/0957-4166(94)80016-2

Reference yield:

: 6920-22-5
Hexane-1,2-diol

: 156599-77-8
(2R,6S,7R,9R,14S)-14-Benzyloxymethyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

: 56552-80-8
(R)-3-benzyloxy-1,2-propanediol

: 156599-71-2
(2R,6S,7R,9R,14S)-14-tert-Butyl-2,9-diphenyl-1,8,13,16-tetraoxa-dispiro[5.0.5.4]hexadecane

Guidance literature:: With camphor-10-sulfonic acid; In toluene; at 110 ℃; Yield given. Yields of byproduct given;
DOI:10.1016/0957-4166(94)80016-2