(R)-N-((3R,4S)-3-hydroxy-3-phenyl-3,4-dihydro-2H-chromen-4-yl)tert-butylsulfinamide

Base Information

Chemical Name:(R)-N-((3R,4S)-3-hydroxy-3-phenyl-3,4-dihydro-2H-chromen-4-yl)tert-butylsulfinamide
CAS No.:1574474-96-6
Molecular Formula:C₁₉H₂₃NO₃S
Molecular Weight:345.463
Hs Code.:

Synonyms:(R)-N-((3R,4S)-3-hydroxy-3-phenyl-3,4-dihydro-2H-chromen-4-yl)tert-butylsulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-N-((3R,4S)-3-hydroxy-3-phenyl-3,4-dihydro-2H-chromen-4-yl)tert-butylsulfinamide

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Technology Process of (R)-N-((3R,4S)-3-hydroxy-3-phenyl-3,4-dihydro-2H-chromen-4-yl)tert-butylsulfinamide

There total 4 articles about (R)-N-((3R,4S)-3-hydroxy-3-phenyl-3,4-dihydro-2H-chromen-4-yl)tert-butylsulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1574474-95-5
C₁₉H₂₁NO₃S

: 1574474-96-6
(R)-N-((3R,4S)-3-hydroxy-3-phenyl-3,4-dihydro-2H-chromen-4-yl)tert-butylsulfinamide

Guidance literature:: With samarium diiodide; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1080/00397911.2013.841938

Reference yield:

: 90-02-8
salicylaldehyde

: 1574474-96-6
(R)-N-((3R,4S)-3-hydroxy-3-phenyl-3,4-dihydro-2H-chromen-4-yl)tert-butylsulfinamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium iodide; potassium carbonate / acetone

2: potassium hydrogensulfate / toluene

3: samarium diiodide / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

With potassium hydrogensulfate; samarium diiodide; potassium carbonate; potassium iodide; In tetrahydrofuran; acetone; toluene;
DOI:10.1080/00397911.2013.841938

Reference yield:

: 945656-60-0
2-(2-oxo-2-phenylethoxy)benzaldehyde

: 1574474-96-6
(R)-N-((3R,4S)-3-hydroxy-3-phenyl-3,4-dihydro-2H-chromen-4-yl)tert-butylsulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydrogensulfate / toluene

2: samarium diiodide / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

With potassium hydrogensulfate; samarium diiodide; In tetrahydrofuran; toluene;
DOI:10.1080/00397911.2013.841938