5-(1,2-diacetoxy-ethyl)-1-phenyl-1H-pyrazole-3-carbaldehyde acetyl-phenyl-hydrazone

Base Information

Chemical Name:5-(1,2-diacetoxy-ethyl)-1-phenyl-1H-pyrazole-3-carbaldehyde acetyl-phenyl-hydrazone
CAS No.:3082-92-6
Molecular Formula:C₂₄H₂₄N₄O₅
Molecular Weight:448.478
Hs Code.:

5-(1,2-diacetoxy-ethyl)-1-phenyl-1<i>H</i>-pyrazole-3-carbaldehyde acetyl-phenyl-hydrazone

Synonyms:5-(1,2-diacetoxy-ethyl)-1-phenyl-1H-pyrazole-3-carbaldehyde acetyl-phenyl-hydrazone

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Chemical Property of 5-(1,2-diacetoxy-ethyl)-1-phenyl-1H-pyrazole-3-carbaldehyde acetyl-phenyl-hydrazone

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Technology Process of 5-(1,2-diacetoxy-ethyl)-1-phenyl-1H-pyrazole-3-carbaldehyde acetyl-phenyl-hydrazone

There total 6 articles about 5-(1,2-diacetoxy-ethyl)-1-phenyl-1H-pyrazole-3-carbaldehyde acetyl-phenyl-hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 108-24-7
acetic anhydride

: 534-97-4
glucosazone

: 3082-92-6
5-(1,2-diacetoxy-ethyl)-1-phenyl-1H-pyrazole-3-carbaldehyde acetyl-phenyl-hydrazone

Guidance literature:: for 0.666667h; Heating;
DOI:10.1016/S0008-6215(98)00137-2

Reference yield: 70.0%

: 102918-98-9
3,4,5,6-tetra-O-acetyl-D-lyxo-hexosulose 1-acetylphenylhydrazone 2-phenylhydrazone

: 3082-92-6,102918-97-8,103000-99-3,103405-38-5
(D-glycero-1,2-diacetoxyethyl)-3-formyl-1-phenylpyrazole acetylphenylhydrazone

Guidance literature:: With sodium acetate; acetic anhydride; for 2h; Heating;
DOI:10.1016/0008-6215(85)85007-2

Reference yield:

: 50-99-7
D-glucose

: 3082-92-6
5-(1,2-diacetoxy-ethyl)-1-phenyl-1H-pyrazole-3-carbaldehyde acetyl-phenyl-hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / HOAc / 2 h / 100 °C

2: 77 percent / 0.67 h / Heating

With acetic acid;
DOI:10.1016/S0008-6215(98)00137-2