3-PIPERIDINONE, 1-METHYL-4-(2,4,6-TRIMETHOXYPHENYL)-

Base Information

Chemical Name:3-PIPERIDINONE, 1-METHYL-4-(2,4,6-TRIMETHOXYPHENYL)-
CAS No.:113225-10-8
Molecular Formula:C15H21 N O4
Molecular Weight:279.336
Hs Code.:2933399090
Mol file:113225-10-8.mol

Synonyms:3-PIPERIDINONE, 1-METHYL-4-(2,4,6-TRIMETHOXYPHENYL)-;N-METHYL-3-OXO-4-(2’,4’,6’-TRIMETHOXY) PIPERIDINE

Suppliers and Price of 3-PIPERIDINONE, 1-METHYL-4-(2,4,6-TRIMETHOXYPHENYL)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-Methyl-4-(2,4,6-trimethoxyphenyl)piperidin-3-one
100mg
$ 60.00

Crysdot
1-Methyl-4-(2,4,6-trimethoxyphenyl)piperidin-3-one 95+%
100g
$ 2451.00

Crysdot
1-Methyl-4-(2,4,6-trimethoxyphenyl)piperidin-3-one 95+%
25g
$ 980.00

Crysdot
1-Methyl-4-(2,4,6-trimethoxyphenyl)piperidin-3-one 95+%
5g
$ 297.00

Crysdot
1-Methyl-4-(2,4,6-trimethoxyphenyl)piperidin-3-one 95+%
10g
$ 495.00

Chemenu
1-Methyl-4-(2,4,6-trimethoxyphenyl)piperidin-3-one 95%
1g
$ 102.00

Chemenu
1-Methyl-4-(2,4,6-trimethoxyphenyl)piperidin-3-one 95%
10g
$ 468.00

Chemenu
1-Methyl-4-(2,4,6-trimethoxyphenyl)piperidin-3-one 95%
5g
$ 281.00

Chemenu
1-Methyl-4-(2,4,6-trimethoxyphenyl)piperidin-3-one 95%
25g
$ 926.00

American Custom Chemicals Corporation
N-METHYL-3-OXO-4-(2',4',6'-TRIMETHOXYPHENYL) PIPERIDINE 95.00%
50MG
$ 885.31

Total 8 raw suppliers

Chemical Property of 3-PIPERIDINONE, 1-METHYL-4-(2,4,6-TRIMETHOXYPHENYL)-

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Melting Point:110-112 °C
Refractive Index:1.519
Boiling Point:405°Cat760mmHg
PKA:6.46±0.40(Predicted)
Flash Point:198.7°C
PSA：48.00000
Density:1.116g/cm³
LogP:1.63850
Storage Temp.:Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

1-Methyl-4-(2,4,6-trimethoxyphenyl)piperidin-3-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-PIPERIDINONE, 1-METHYL-4-(2,4,6-TRIMETHOXYPHENYL)-

There total 6 articles about 3-PIPERIDINONE, 1-METHYL-4-(2,4,6-TRIMETHOXYPHENYL)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 113225-08-4,113225-12-0,113225-18-6,113225-19-7,117955-02-9,234771-34-7
(±)-trans-1-methyl-4-(2,4,6-trimethoxyphenyl)piperidin-3-ol

: 113225-10-8
(+)-1-Methyl-4-(2,4,6-trimethoxyphenyl)-piperidin-3-one

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; 1.) -60 deg C, 15 min; 2.) up to -30 deg C;
DOI:10.1016/S0040-4020(01)90352-7

Reference yield:

: 79-37-8
oxalyl dichloride

: 234771-34-7
trans-3-hydroxy-4-(2,4,6-trimethoxyphenyl)-1-methylpiperidine

: 113225-10-8
(+)-1-Methyl-4-(2,4,6-trimethoxyphenyl)-piperidin-3-one

Guidance literature:: With dimethyl sulfoxide; triethylamine; In dichloromethane;

Reference yield:

: 1445-73-4
1-Methyl-4-piperidone

: 113225-10-8
(+)-1-Methyl-4-(2,4,6-trimethoxyphenyl)-piperidin-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / HCl / acetic acid / 1.) 25 deg C, 1 h; 2.) 95-100 deg C, 3 h

2: 70 percent / 1.) boron trifluoride etherate, sodium borohydride; 2.) conc. HCl, 30 percent hydrogen peroxide / tetrahydrofuran; H₂O / 1.) 50 deg C, 1 h, up to 0 deg C; 2.) 50 deg C, 2 h

3: 76 percent / dimethylsulfoxide, triethylamine, oxalyl chloride / CH₂Cl₂ / 1.) -60 deg C, 15 min; 2.) up to -30 deg C

With hydrogenchloride; sodium tetrahydroborate; oxalyl dichloride; boron trifluoride diethyl etherate; dihydrogen peroxide; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; water; acetic acid;
DOI:10.1016/S0040-4020(01)90352-7