Technology Process of C34H35N3O4S
There total 9 articles about C34H35N3O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: aluminum (III) chloride / dichloromethane / 0 °C / Inert atmosphere
2: nitro acetate / dichloromethane / 2.17 h / -20 - 20 °C / Inert atmosphere
3: dihydrogen peroxide; acetic acid / water / 2 h / Reflux
4: palladium 10% on activated carbon; hydrogen; acetic acid / water / 60 °C
5: pyridine / 0.5 h / 0 °C / Inert atmosphere
With
pyridine; aluminum (III) chloride; nitro acetate; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; acetic acid;
In
dichloromethane; water;
DOI:10.1016/j.tet.2012.06.070
- Guidance literature:
-
Multi-step reaction with 4 steps
1: nitro acetate / dichloromethane / 2.17 h / -20 - 20 °C / Inert atmosphere
2: dihydrogen peroxide; acetic acid / water / 2 h / Reflux
3: palladium 10% on activated carbon; hydrogen; acetic acid / water / 60 °C
4: pyridine / 0.5 h / 0 °C / Inert atmosphere
With
pyridine; nitro acetate; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; acetic acid;
In
dichloromethane; water;
DOI:10.1016/j.tet.2012.06.070