2-(3-Methoxy-4-bromophenyl)ethylamine

Base Information

Chemical Name:2-(3-Methoxy-4-bromophenyl)ethylamine
CAS No.:113081-51-9
Molecular Formula:C₉H₁₂BrNO
Molecular Weight:230.104
Hs Code.:2922199090
DSSTox Substance ID:DTXSID10603142
Wikidata:Q82500421
Mol file:113081-51-9.mol

Synonyms:113081-51-9;2-(3-METHOXY-4-BROMOPHENYL)ETHYLAMINE;2-(4-Bromo-3-methoxyphenyl)ethanamine;Benzeneethanamine,4-bromo-3-methoxy-;Benzeneethanamine, 4-bromo-3-methoxy-;SCHEMBL153912;4-Bromo-3-methoxyphenethylamine;4-bromo-3-methoxyphenethyl amine;DTXSID10603142;KNLHFRSNELASBY-UHFFFAOYSA-N;MFCD11053672;AKOS022931443;2-(4-bromo-3-methoxy-phenyl)-ethylamine;AS-37966;2-(4-Bromo-3-methoxyphenyl)ethan-1-amine;A907395

Suppliers and Price of 2-(3-Methoxy-4-bromophenyl)ethylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-(3-Methoxy-4-bromophenyl)ethylamine
50mg
$ 175.00

AstaTech
2-(3-METHOXY-4-BROMOPHENYL)ETHYLAMINE 97%
1 / G
$ 588.00

AstaTech
2-(3-METHOXY-4-BROMOPHENYL)ETHYLAMINE 97%
0.25 / G
$ 235.00

AK Scientific
2-(3-Methoxy-4-bromophenyl)ethylamine
1g
$ 868.00

Total 12 raw suppliers

Chemical Property of 2-(3-Methoxy-4-bromophenyl)ethylamine

Chemical Property:

Boiling Point:303.2±27.0 °C(Predicted)
PKA:9.61±0.10(Predicted)
PSA：35.25000
Density:1.385±0.06 g/cm3(Predicted)
LogP:2.65920
XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:229.01023
Heavy Atom Count:12
Complexity:132

Purity/Quality:

97% ^*data from raw suppliers

2-(3-Methoxy-4-bromophenyl)ethylamine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=CC(=C1)CCN)Br

Technology Process of 2-(3-Methoxy-4-bromophenyl)ethylamine

There total 7 articles about 2-(3-Methoxy-4-bromophenyl)ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1177015-72-3
1-bromo-2-methoxy-4-((E)-2-nitro-vinyl)-benzene

: 113081-51-9
2-(4-bromo-3-methoxy-phenyl)-ethylamine

Guidance literature:: 1-bromo-2-methoxy-4-((E)-2-nitro-vinyl)-benzene; With methanol; sodium tetrahydroborate; at 0 - 20 ℃; for 1h;

With ammonium chloride; acetic acid; zinc; In water; at 50 ℃; for 1h;

Reference yield:

: 90151-40-9
4-amino-3-methoxybenzaldehyde

: 113081-51-9
2-(4-bromo-3-methoxy-phenyl)-ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-Butyl nitrite; copper(I) bromide / acetonitrile / 12 h / 20 °C

2.1: acetic acid; ammonium acetate / 12 h / 80 °C

3.1: sodium tetrahydroborate; methanol / 1 h / 0 - 20 °C

3.2: 1 h / 50 °C

With methanol; sodium tetrahydroborate; n-Butyl nitrite; ammonium acetate; acetic acid; copper(I) bromide; In acetonitrile;

Reference yield:

: 1-bromo-2-methoxy-4-(2-nitrovinyl)benzene

: 113081-51-9
2-(4-bromo-3-methoxy-phenyl)-ethylamine

Guidance literature:: 1-bromo-2-methoxy-4-(2-nitrovinyl)benzene; With borane-THF; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

With sodium tetrahydroborate; In tetrahydrofuran; at 65 ℃; for 18h; Inert atmosphere;