C₁₄H₁₇N₃O₄

Base Information

• Chemical Name: C₁₄H₁₇N₃O₄
• CAS No.: 1469300-42-2
• Molecular Formula: C₁₄H₁₇N₃O₄
• Molecular Weight: 291.307
• Mol file: 1469300-42-2.mol

Synonyms:C₁₄H₁₇N₃O₄

Chemical Property of C₁₄H₁₇N₃O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₁₇N₃O₄

There total 2 articles about C₁₄H₁₇N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

methanol (67-56-1) + C13H14N4O2 (1469300-41-1) → C14H17N3O4 (1469300-42-2)

Guidance literature:

With acetyl chloride; at 0 - 50 ℃; for 4.5h; Inert atmosphere;

DOI:10.1002/anie.201304239

Reference yield:

C13H17N3O3 → C14H17N3O4 (1469300-42-2)

Guidance literature:

Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / acetonitrile / 0.17 h / 0 °C / Inert atmosphere

2: acetyl chloride / 4.5 h / 0 - 50 °C / Inert atmosphere

With boron trifluoride diethyl etherate; acetyl chloride; In acetonitrile;

DOI:10.1002/anie.201304239

Reference yield: 86.0%

di-tert-butyl dicarbonate (24424-99-5) + C14H17N3O4 (1469300-42-2) → C19H27NO6 (1469300-34-2)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethyl acetate; for 6h; under 760.051 Torr;

DOI:10.1002/anie.201304239

upstream raw materials:

methanol

C₁₃H₁₄N₄O₂

Downstream raw materials:

C₂₅H₃₅N₅O₈

C₄₄H₅₈N₁₀O₁₃

C₁₈H₂₅NO₆

C₂₀H₂₇N₅O₆