2-(2,6-dimethylphenyl)-4-methoxy-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidine

Base Information

Chemical Name:2-(2,6-dimethylphenyl)-4-methoxy-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidine
CAS No.:1421253-29-3
Molecular Formula:C₁₆H₁₉N₃O
Molecular Weight:269.346
Hs Code.:

Synonyms:2-(2,6-dimethylphenyl)-4-methoxy-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidine

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Chemical Property of 2-(2,6-dimethylphenyl)-4-methoxy-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidine

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Technology Process of 2-(2,6-dimethylphenyl)-4-methoxy-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidine

There total 3 articles about 2-(2,6-dimethylphenyl)-4-methoxy-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421253-28-2
6-benzyl-2-(2,6-dimethylphenyl)-4-methoxy-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidine

: 1421253-29-3
2-(2,6-dimethylphenyl)-4-methoxy-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidine

Guidance literature:: With 20% palladium hydroxide-activated charcoal; hydrogen; acetic acid; In tetrahydrofuran; water; at 20 - 40 ℃; for 16.5h; Inert atmosphere;

Reference yield:

: 1421067-10-8
6-benzyl-2-chloro-4-methoxy-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidine

: 1421253-29-3
2-(2,6-dimethylphenyl)-4-methoxy-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; 1,2-dimethoxyethane / 48 h / 100 °C / Inert atmosphere

2: acetic acid; 20% palladium hydroxide-activated charcoal; hydrogen / water; tetrahydrofuran / 16.5 h / 20 - 40 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 20% palladium hydroxide-activated charcoal; hydrogen; sodium carbonate; acetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; water;

Reference yield:

: 778574-06-4
6-benzyl-2,4-dichloro-5,6,7,8-tetrahydropyrido[4,3-d]-pyrimidine

: 1421253-29-3
2-(2,6-dimethylphenyl)-4-methoxy-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 0.75 h / 0 - 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; 1,2-dimethoxyethane / 48 h / 100 °C / Inert atmosphere

3: acetic acid; 20% palladium hydroxide-activated charcoal; hydrogen / water; tetrahydrofuran / 16.5 h / 20 - 40 °C / Inert atmosphere

With methanol; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 20% palladium hydroxide-activated charcoal; hydrogen; sodium carbonate; acetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; water;