N¹-(4-chlorophenyl)-N²-(5-fluoro-2,4-dinitrophenyl)benzene-1,2-diamine

Base Information

Chemical Name:N¹-(4-chlorophenyl)-N²-(5-fluoro-2,4-dinitrophenyl)benzene-1,2-diamine
CAS No.:1332634-91-9
Molecular Formula:C₁₈H₁₂ClFN₄O₄
Molecular Weight:402.769
Hs Code.:

N<SUP>1</SUP>-(4-chlorophenyl)-N<SUP>2</SUP>-(5-fluoro-2,4-dinitrophenyl)benzene-1,2-diamine

Synonyms:N¹-(4-chlorophenyl)-N²-(5-fluoro-2,4-dinitrophenyl)benzene-1,2-diamine

Suppliers and Price of N¹-(4-chlorophenyl)-N²-(5-fluoro-2,4-dinitrophenyl)benzene-1,2-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of N¹-(4-chlorophenyl)-N²-(5-fluoro-2,4-dinitrophenyl)benzene-1,2-diamine

Chemical Property:

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of N¹-(4-chlorophenyl)-N²-(5-fluoro-2,4-dinitrophenyl)benzene-1,2-diamine

There total 3 articles about N¹-(4-chlorophenyl)-N²-(5-fluoro-2,4-dinitrophenyl)benzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 327-92-4
1,5-difluoro-2,4-dinitrobenzene

: 68817-71-0
2-(4-chloroanilino)aniline

: 1332634-91-9
N¹-(4-chlorophenyl)-N²-(5-fluoro-2,4-dinitrophenyl)benzene-1,2-diamine

Guidance literature:: In ethanol; at 20 ℃; for 1.5h;
DOI:10.1016/j.bmc.2014.11.028

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 1332634-91-9
N¹-(4-chlorophenyl)-N²-(5-fluoro-2,4-dinitrophenyl)benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium fluoride; potassium carbonate / 10 h / 160 °C

2: acetic acid; zinc / dichloromethane / 4 h / 20 °C

3: triethylamine / methanol / 5 h / Reflux

With potassium fluoride; potassium carbonate; acetic acid; triethylamine; zinc; In methanol; dichloromethane;
DOI:10.3390/molecules17044545

Reference yield:

: 23008-56-2
N-(4-chlorophenyl)-2-nitroaniline

: 1332634-91-9
N¹-(4-chlorophenyl)-N²-(5-fluoro-2,4-dinitrophenyl)benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; zinc / dichloromethane / 4 h / 20 °C

2: triethylamine / methanol / 5 h / Reflux

With acetic acid; triethylamine; zinc; In methanol; dichloromethane;
DOI:10.3390/molecules17044545