C₅₄H₈₁BrO₈Si₃

Base Information

Chemical Name:C₅₄H₈₁BrO₈Si₃
CAS No.:223260-50-2
Molecular Formula:C₅₄H₈₁BrO₈Si₃
Molecular Weight:1022.39
Hs Code.:

C<sub>54</sub>H<sub>81</sub>BrO<sub>8</sub>Si<sub>3</sub>

Synonyms:C₅₄H₈₁BrO₈Si₃

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Chemical Property of C₅₄H₈₁BrO₈Si₃

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Technology Process of C₅₄H₈₁BrO₈Si₃

There total 4 articles about C₅₄H₈₁BrO₈Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 223260-49-9
C₅₄H₈₃BrO₈Si₃

: 223260-50-2
C₅₄H₈₁BrO₈Si₃

Guidance literature:: With chromic acid; In diethyl ether; dichloromethane; for 0.25h;
DOI:10.1021/ja9817139

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 223260-50-2
C₅₄H₈₁BrO₈Si₃

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / imidazole / dimethylformamide / 5 h

2: 95 percent / KHCO₃ / methanol; H₂O

3: 97 percent / H₂CrO₄ / diethyl ether; CH₂Cl₂ / 0.25 h

With 1H-imidazole; chromic acid; potassium hydrogencarbonate; In methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja9817139

Reference yield:

: 164530-22-7
C₅₀H₇₁BrO₉Si₂

: 223260-50-2
C₅₄H₈₁BrO₈Si₃

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / imidazole / dimethylformamide / 5 h

2: 95 percent / KHCO₃ / methanol; H₂O

3: 97 percent / H₂CrO₄ / diethyl ether; CH₂Cl₂ / 0.25 h

With 1H-imidazole; chromic acid; potassium hydrogencarbonate; In methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja9817139