3-(3,4-Dimethoxy-phenyl)-6,7-dimethoxy-2-(2-phenylsulfanyl-ethyl)-1,2,3,4-tetrahydro-isoquinoline

Base Information

Chemical Name:3-(3,4-Dimethoxy-phenyl)-6,7-dimethoxy-2-(2-phenylsulfanyl-ethyl)-1,2,3,4-tetrahydro-isoquinoline
CAS No.:148679-68-9
Molecular Formula:C₂₇H₃₁NO₄S
Molecular Weight:465.613
Hs Code.:

Synonyms:3-(3,4-Dimethoxy-phenyl)-6,7-dimethoxy-2-(2-phenylsulfanyl-ethyl)-1,2,3,4-tetrahydro-isoquinoline

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Chemical Property of 3-(3,4-Dimethoxy-phenyl)-6,7-dimethoxy-2-(2-phenylsulfanyl-ethyl)-1,2,3,4-tetrahydro-isoquinoline

Chemical Property:

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Technology Process of 3-(3,4-Dimethoxy-phenyl)-6,7-dimethoxy-2-(2-phenylsulfanyl-ethyl)-1,2,3,4-tetrahydro-isoquinoline

There total 5 articles about 3-(3,4-Dimethoxy-phenyl)-6,7-dimethoxy-2-(2-phenylsulfanyl-ethyl)-1,2,3,4-tetrahydro-isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 148679-64-5
[1,2-Bis-(3,4-dimethoxy-phenyl)-ethyl]-(2-phenylsulfanyl-ethyl)-amine

: 148679-68-9
3-(3,4-Dimethoxy-phenyl)-6,7-dimethoxy-2-(2-phenylsulfanyl-ethyl)-1,2,3,4-tetrahydro-isoquinoline

Guidance literature:: With hydrogenchloride; In methanol; Heating;
DOI:10.3987/COM-92-S14

Reference yield:

: 2014-75-7
2-(phenylthio)ethanamine

: 148679-68-9
3-(3,4-Dimethoxy-phenyl)-6,7-dimethoxy-2-(2-phenylsulfanyl-ethyl)-1,2,3,4-tetrahydro-isoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: p-TsOH / benzene / Heating

2: NaBH₄ / methanol / 5 h / Ambient temperature

3: 78 percent / aq. HCl / methanol / Heating

With hydrogenchloride; sodium tetrahydroborate; toluene-4-sulfonic acid; In methanol; benzene;
DOI:10.3987/COM-92-S14

Reference yield:

: 41010-04-2
4-nitro-2-(2-(phenylthio)ethyl)isoindoline-1,3-dione

: 148679-68-9
3-(3,4-Dimethoxy-phenyl)-6,7-dimethoxy-2-(2-phenylsulfanyl-ethyl)-1,2,3,4-tetrahydro-isoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: NH₂NH₂*H₂O / ethanol / 1 h / Heating

2: p-TsOH / benzene / Heating

3: NaBH₄ / methanol / 5 h / Ambient temperature

4: 78 percent / aq. HCl / methanol / Heating

With hydrogenchloride; sodium tetrahydroborate; toluene-4-sulfonic acid; hydrazine hydrate; In methanol; ethanol; benzene;
DOI:10.3987/COM-92-S14