(3S)-5-tert-butyldimethylsilyloxy-3-(4-methoxybenzyloxy)-4,4-dimethylpentanal

Base Information

Chemical Name:(3S)-5-tert-butyldimethylsilyloxy-3-(4-methoxybenzyloxy)-4,4-dimethylpentanal
CAS No.:935248-45-6
Molecular Formula:C₂₁H₃₆O₄Si
Molecular Weight:380.6
Hs Code.:

Synonyms:(3S)-5-tert-butyldimethylsilyloxy-3-(4-methoxybenzyloxy)-4,4-dimethylpentanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S)-5-tert-butyldimethylsilyloxy-3-(4-methoxybenzyloxy)-4,4-dimethylpentanal

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Technology Process of (3S)-5-tert-butyldimethylsilyloxy-3-(4-methoxybenzyloxy)-4,4-dimethylpentanal

There total 10 articles about (3S)-5-tert-butyldimethylsilyloxy-3-(4-methoxybenzyloxy)-4,4-dimethylpentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 935248-44-5
5-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-4,4-dimethyl-pentan-1-ol

: 935248-45-6
(3S)-5-tert-butyldimethylsilyloxy-3-(4-methoxybenzyloxy)-4,4-dimethylpentanal

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; for 2h; Inert atmosphere;
DOI:10.1021/ol100515m

Reference yield: 87.0%

: 1103774-80-6
C₂₂H₃₈O₃Si

: 935248-45-6
(3S)-5-tert-butyldimethylsilyloxy-3-(4-methoxybenzyloxy)-4,4-dimethylpentanal

Guidance literature:: With 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; In 1,4-dioxane; water; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/ja105129p

Reference yield: 70.0%

: 935248-44-5
5-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-4,4-dimethyl-pentan-1-ol

: 935248-45-6
(3S)-5-tert-butyldimethylsilyloxy-3-(4-methoxybenzyloxy)-4,4-dimethylpentanal

: C₁₃H₂₆O₂Si

Guidance literature:: With sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; In dichloromethane; at 0 - 20 ℃; for 1.75h; Inert atmosphere;
DOI:10.1016/j.tet.2020.131743