2,4,6-trimethylphenylphenylphosphine oxide

Base Information

Chemical Name:2,4,6-trimethylphenylphenylphosphine oxide
CAS No.:98934-20-4
Molecular Formula:C₁₅H₁₇OP
Molecular Weight:244.273
Hs Code.:

Synonyms:2,4,6-trimethylphenylphenylphosphine oxide

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Chemical Property of 2,4,6-trimethylphenylphenylphosphine oxide

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Technology Process of 2,4,6-trimethylphenylphenylphosphine oxide

There total 12 articles about 2,4,6-trimethylphenylphenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.5%

: 644-97-3
Dichlorophenylphosphine

: 108-67-8
1,3,5-trimethyl-benzene

: 98934-20-4
2,4,6-trimethylphenylphenylphosphine oxide

Guidance literature:: Dichlorophenylphosphine; 1,3,5-trimethyl-benzene; With aluminum (III) chloride; at 90 ℃; for 12h; Inert atmosphere;

With water; for 4.5h; Cooling with ice;

Reference yield: 93.0%

: 1061745-76-3
(-)-menthyl (Rp)-mesitylphosphinate

: 591-51-5
phenyllithium

: 98934-20-4,1061745-96-7,1061746-09-5
(Sp)-mesitylphenylphosphine oxide

Guidance literature:: In diethyl ether; at -80 ℃; for 17h; optical yield given as %ee; Inert atmosphere;
DOI:10.1021/ja804412k

Reference yield: 30.0%

: 217975-66-1
phenyl(2,4,6-trimethyl)phosphine

: 844-51-9
2,5-diphenyl-p-benzoquinone

: 1579997-16-2
C₃₃H₂₉O₃P

: 98934-20-4
2,4,6-trimethylphenylphenylphosphine oxide

Guidance literature:: phenyl(2,4,6-trimethyl)phosphine; With C₁₈H₂₂N₃Pd⁽¹⁺⁾*ClO₄^(1-); In chloroform; at 20 ℃; for 0.0333333h; Inert atmosphere; Schlenk technique;

2,5-diphenyl-p-benzoquinone; With triethylamine; In chloroform; at -45 ℃; for 10h; Inert atmosphere; Schlenk technique;

With 3-chloro-benzenecarboperoxoic acid; In chloroform; at -45 ℃; for 8h; enantioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/ja501007t