oxanthrene-1-carbonitrile

Base Information

Chemical Name:oxanthrene-1-carbonitrile
CAS No.:234113-43-0
Molecular Formula:C₁₃H₇NO₂
Molecular Weight:209.204
Hs Code.:

Synonyms:1-cyanodibenzo[1,4]dioxine

Suppliers and Price of oxanthrene-1-carbonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of oxanthrene-1-carbonitrile

Chemical Property:

Vapor Pressure:3.82E-05mmHg at 25°C

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

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Technology Process of oxanthrene-1-carbonitrile

There total 1 articles about oxanthrene-1-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 21524-39-0
2,3-difluorobenzonitrile

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 3-fluoro-2-(2-hydroxy-phenoxy)-benzonitrile

: C₂₀H₁₀F₂N₂O₂

: 234113-43-0
1-cyanodibenzo[1,4]dioxine

Guidance literature:: In dimethyl sulfoxide; at 20 ℃; for 120h;
DOI:10.1039/b008503k

Reference yield: 100.0%

: 234113-43-0
1-cyanodibenzo[1,4]dioxine

: 51689-36-2
dibenzo<1,4>dioxin-1-carboxylic acid

Guidance literature:: With potassium hydroxide; In water; ethylene glycol; for 0.5h; Heating;
DOI:10.1039/b008508l

Reference yield:

: 234113-43-0
1-cyanodibenzo[1,4]dioxine

: N-(4-amino-3,4-dioxo-1-phenylbutan-2-yl)dibenzo[b,e][1,4]dioxine-1-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide; water / ethylene glycol / 12 h / 130 °C

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 15 °C

3: Dess-Martin periodane / dimethyl sulfoxide; dichloromethane / 1 h / 15 °C

With water; Dess-Martin periodane; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In dichloromethane; ethylene glycol; dimethyl sulfoxide; N,N-dimethyl-formamide;