C₁₁H₉IN₂OS

Base Information

Chemical Name:C₁₁H₉IN₂OS
CAS No.:1420830-24-5
Molecular Formula:C₁₁H₉IN₂OS
Molecular Weight:344.176
Hs Code.:

C<sub>11</sub>H<sub>9</sub>IN<sub>2</sub>OS

Synonyms:C₁₁H₉IN₂OS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁H₉IN₂OS

Chemical Property:

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Technology Process of C₁₁H₉IN₂OS

There total 4 articles about C₁₁H₉IN₂OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1383546-18-6
5-iodo-3-methylisothiazole-4-carboxylic acid

: 62-53-3
aniline

: 1420830-24-5
C₁₁H₉IN₂OS

Guidance literature:: 5-iodo-3-methylisothiazole-4-carboxylic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 2h;

aniline; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 1420625-84-8
methyl 3-amino-2-thioformylbut-2-enoate

: 1420830-24-5
C₁₁H₉IN₂OS

Guidance literature:: Multi-step reaction with 4 steps

1.1: 3-chloro-benzenecarboperoxoic acid / ethanol / 3 h / Reflux

2.1: water; sodium hydroxide / tetrahydrofuran; methanol / 16 h / 40 °C

3.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

3.2: 1 h / 20 °C

4.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 2 h / 20 °C

4.2: 1 h / 20 °C

With n-butyllithium; oxalyl dichloride; water; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane;

Reference yield:

: 74410-97-2
methyl 3-methylisothiazole-4-carboxylate

: 1420830-24-5
C₁₁H₉IN₂OS

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; sodium hydroxide / tetrahydrofuran; methanol / 16 h / 40 °C

2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 1 h / 20 °C

3.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 2 h / 20 °C

3.2: 1 h / 20 °C

With n-butyllithium; oxalyl dichloride; water; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;