(S,E)-(8-amino-3-(hydroxymethyl)-6,10-dioxo-2-oxa-5,7,9-triazahentriacont-7-en-1-yl)phosphonic acid

Base Information

Chemical Name:(S,E)-(8-amino-3-(hydroxymethyl)-6,10-dioxo-2-oxa-5,7,9-triazahentriacont-7-en-1-yl)phosphonic acid
CAS No.:1608459-53-5
Molecular Formula:C₂₈H₅₇N₄O₇P
Molecular Weight:592.757
Hs Code.:

Synonyms:(S,E)-(8-amino-3-(hydroxymethyl)-6,10-dioxo-2-oxa-5,7,9-triazahentriacont-7-en-1-yl)phosphonic acid

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Chemical Property of (S,E)-(8-amino-3-(hydroxymethyl)-6,10-dioxo-2-oxa-5,7,9-triazahentriacont-7-en-1-yl)phosphonic acid

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Technology Process of (S,E)-(8-amino-3-(hydroxymethyl)-6,10-dioxo-2-oxa-5,7,9-triazahentriacont-7-en-1-yl)phosphonic acid

There total 2 articles about (S,E)-(8-amino-3-(hydroxymethyl)-6,10-dioxo-2-oxa-5,7,9-triazahentriacont-7-en-1-yl)phosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2857-97-8
trimethylsilyl bromide

: 1608457-43-7
1-(2S)-2-[(diisopropoxyphosphoryl)methoxy-3-(triphenylmethoxy)propyl-N⁴-docosanoyl-5-azacytosine]

: 1608459-53-5
(S,E)-(8-amino-3-(hydroxymethyl)-6,10-dioxo-2-oxa-5,7,9-triazahentriacont-7-en-1-yl)phosphonic acid

: 124-26-5
stearamide

Guidance literature:: In acetonitrile; at 20 ℃; for 24h;
DOI:10.1016/j.bmc.2014.03.031

Reference yield:

: 933460-58-3
1-{(2S)-2-[(diisopropoxyphosphoryl)methoxy-3-(triphenylmethoxy)]propyl}-5-azacytosine

: 21132-76-3
docosanoyl chloride

: 1608459-53-5
(S,E)-(8-amino-3-(hydroxymethyl)-6,10-dioxo-2-oxa-5,7,9-triazahentriacont-7-en-1-yl)phosphonic acid

: 124-26-5
stearamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 48 h / 20 °C

2: acetonitrile / 24 h / 20 °C

In pyridine; acetonitrile;
DOI:10.1016/j.bmc.2014.03.031