1-lithiomethyl phenyl selenoxide

Base Information

Chemical Name:1-lithiomethyl phenyl selenoxide
CAS No.:85662-39-1
Molecular Formula:C₇H₇LiOSe
Molecular Weight:193.033
Hs Code.:

Synonyms:1-lithiomethyl phenyl selenoxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-lithiomethyl phenyl selenoxide

Chemical Property:

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Technology Process of 1-lithiomethyl phenyl selenoxide

There total 2 articles about 1-lithiomethyl phenyl selenoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4346-64-9
selenoanisole

: 85662-39-1
1-lithiomethyl phenyl selenoxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; 1.) -20 deg C, 15 min, 2.) -78 deg C, 10 min;
DOI:10.1021/jo00160a034

Reference yield:

: 1666-13-3
diphenyl diselenide

: 85662-39-1
1-lithiomethyl phenyl selenoxide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / NaBH₄ / ethanol / Heating

2: 1.) m-chloroperbenzoic acid (MCPBA), 2.) lithium diisopropylamide (LDA) / tetrahydrofuran / 1.) -20 deg C, 15 min, 2.) -78 deg C, 10 min

With sodium tetrahydroborate; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; ethanol;
DOI:10.1021/jo00160a034