(R)-methyl-2-methyl-2-(4,5-dihydro-4-isopropyl-2-thiazolyl)propanedithioate

Base Information

Chemical Name:(R)-methyl-2-methyl-2-(4,5-dihydro-4-isopropyl-2-thiazolyl)propanedithioate
CAS No.:420133-87-5
Molecular Formula:C₁₁H₁₉NS₃
Molecular Weight:261.477
Hs Code.:

Synonyms:(R)-methyl-2-methyl-2-(4,5-dihydro-4-isopropyl-2-thiazolyl)propanedithioate

Suppliers and Price of (R)-methyl-2-methyl-2-(4,5-dihydro-4-isopropyl-2-thiazolyl)propanedithioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-methyl-2-methyl-2-(4,5-dihydro-4-isopropyl-2-thiazolyl)propanedithioate

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Technology Process of (R)-methyl-2-methyl-2-(4,5-dihydro-4-isopropyl-2-thiazolyl)propanedithioate

There total 1 articles about (R)-methyl-2-methyl-2-(4,5-dihydro-4-isopropyl-2-thiazolyl)propanedithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4276-09-9,473-75-6
(R)-2-amino-3-methylbutanol

: 420133-87-5
(R)-methyl-2-methyl-2-(4,5-dihydro-4-isopropyl-2-thiazolyl)propanedithioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 98 percent / Et₃N / 12 h / 20 °C

2.1: 98 percent / mesylchloride; Et₃N / tetrahydrofuran / 0.17 h / 20 °C

3.1: t-BuLi / tetrahydrofuran; cyclohexane / 3 h / -78 °C

3.2: tetrahydrofuran / 2 h / -40 °C

3.3: 83 percent / tetrahydrofuran / 20 °C

With tert.-butyl lithium; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; cyclohexane;
DOI:10.1016/S0957-4166(01)00481-5