1-hexyl 2-acetamido-4,6-O-benzylidene-3-O-cyanomethyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:1-hexyl 2-acetamido-4,6-O-benzylidene-3-O-cyanomethyl-2-deoxy-β-D-glucopyranoside
CAS No.:231607-26-4
Molecular Formula:C₂₃H₃₂N₂O₆
Molecular Weight:432.517
Hs Code.:

Synonyms:1-hexyl 2-acetamido-4,6-O-benzylidene-3-O-cyanomethyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of 1-hexyl 2-acetamido-4,6-O-benzylidene-3-O-cyanomethyl-2-deoxy-β-D-glucopyranoside

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Technology Process of 1-hexyl 2-acetamido-4,6-O-benzylidene-3-O-cyanomethyl-2-deoxy-β-D-glucopyranoside

There total 5 articles about 1-hexyl 2-acetamido-4,6-O-benzylidene-3-O-cyanomethyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 231607-07-1
1-hexyl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 590-17-0
cyanomethyl bromide

: 231607-26-4
1-hexyl 2-acetamido-4,6-O-benzylidene-3-O-cyanomethyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With sodium hydride; In 1,4-dioxane; for 1.5h; Ambient temperature;
DOI:10.1016/S0008-6215(99)00030-0

Reference yield:

: 190912-49-3
hexyl 2-(acetylamino)-2-deoxy-β-D-glucopyranoside

: 231607-26-4
1-hexyl 2-acetamido-4,6-O-benzylidene-3-O-cyanomethyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: ZnCl₂

2: 95 percent / NaH / dioxane / 1.5 h / Ambient temperature

With sodium hydride; zinc(II) chloride; In 1,4-dioxane;
DOI:10.1016/S0008-6215(99)00030-0

Reference yield:

: 172945-26-5
1-hexyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

: 231607-26-4
1-hexyl 2-acetamido-4,6-O-benzylidene-3-O-cyanomethyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: NaOMe, Dowex 50 (H⁺ form) / methanol / 0.5 h / Ambient temperature

2: ZnCl₂

3: 95 percent / NaH / dioxane / 1.5 h / Ambient temperature

With Dowex 50 (H⁺ form); sodium methylate; sodium hydride; zinc(II) chloride; In 1,4-dioxane; methanol;
DOI:10.1016/S0008-6215(99)00030-0