7-(2-acetoxyphenyl)-4-[2-(1-methyl-1H-imidazol-2-yl)-2-oxoethyl]heptyl pivalate

Base Information

Chemical Name:7-(2-acetoxyphenyl)-4-[2-(1-methyl-1H-imidazol-2-yl)-2-oxoethyl]heptyl pivalate
CAS No.:1261270-15-8
Molecular Formula:C₂₆H₃₆N₂O₅
Molecular Weight:456.582
Hs Code.:

Synonyms:7-(2-acetoxyphenyl)-4-[2-(1-methyl-1H-imidazol-2-yl)-2-oxoethyl]heptyl pivalate

Suppliers and Price of 7-(2-acetoxyphenyl)-4-[2-(1-methyl-1H-imidazol-2-yl)-2-oxoethyl]heptyl pivalate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7-(2-acetoxyphenyl)-4-[2-(1-methyl-1H-imidazol-2-yl)-2-oxoethyl]heptyl pivalate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-(2-acetoxyphenyl)-4-[2-(1-methyl-1H-imidazol-2-yl)-2-oxoethyl]heptyl pivalate

There total 3 articles about 7-(2-acetoxyphenyl)-4-[2-(1-methyl-1H-imidazol-2-yl)-2-oxoethyl]heptyl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1261270-03-4
(E)-6-(1-methyl-1H-imidazol-2-yl)-6-oxo-4-hexen-1-yl pivalate

: C₁₉H₂₇BO₂

: 1261270-15-8
7-(2-acetoxyphenyl)-4-[2-(1-methyl-1H-imidazol-2-yl)-2-oxoethyl]heptyl pivalate

Guidance literature:: With potassium tert-butylate; 1,3-bis(2,4,6-trimethylphenyl)-1,3-dihydro-2H-imidazol-2-ylidene; copper(l) chloride; In tetrahydrofuran; at 80 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol102819k

Reference yield:

: 4125-54-6
2-allylphenyl acetate

: 1261270-15-8
7-(2-acetoxyphenyl)-4-[2-(1-methyl-1H-imidazol-2-yl)-2-oxoethyl]heptyl pivalate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 1 h / 60 °C / Inert atmosphere

2: potassium tert-butylate; 1,3-bis(2,4,6-trimethylphenyl)-1,3-dihydro-2H-imidazol-2-ylidene; copper(l) chloride / tetrahydrofuran / 12 h / 80 °C / Inert atmosphere

With potassium tert-butylate; 1,3-bis(2,4,6-trimethylphenyl)-1,3-dihydro-2H-imidazol-2-ylidene; copper(l) chloride; In tetrahydrofuran;
DOI:10.1021/ol102819k

Reference yield:

: 860772-73-2
1-(1-methyl-1H-imidazole-2-yl)-2-(triphenylphosphoranylidene)-ethanone

: 30435-87-1
2,2-dimethylpropionic acid-4-oxo-butyl ester

: 1261270-15-8
7-(2-acetoxyphenyl)-4-[2-(1-methyl-1H-imidazol-2-yl)-2-oxoethyl]heptyl pivalate

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzene / 12 h / 20 °C / Inert atmosphere

1.2: 12 h / -5 °C / Inert atmosphere

2.1: potassium tert-butylate; 1,3-bis(2,4,6-trimethylphenyl)-1,3-dihydro-2H-imidazol-2-ylidene; copper(l) chloride / tetrahydrofuran / 12 h / 80 °C / Inert atmosphere

With potassium tert-butylate; 1,3-bis(2,4,6-trimethylphenyl)-1,3-dihydro-2H-imidazol-2-ylidene; copper(l) chloride; In tetrahydrofuran; benzene; 1.1: Wittig olefination / 1.2: Wittig olefination;
DOI:10.1021/ol102819k