ethyl 3-[4-bromo-1-(2,4-dimethylphenyl)-1H-imidazol-5-yl]-3-oxopropanoate

Base Information

Chemical Name:ethyl 3-[4-bromo-1-(2,4-dimethylphenyl)-1H-imidazol-5-yl]-3-oxopropanoate
CAS No.:868374-18-9
Molecular Formula:C₁₆H₁₇BrN₂O₃
Molecular Weight:365.227
Hs Code.:

Synonyms:ethyl 3-[4-bromo-1-(2,4-dimethylphenyl)-1H-imidazol-5-yl]-3-oxopropanoate

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Chemical Property of ethyl 3-[4-bromo-1-(2,4-dimethylphenyl)-1H-imidazol-5-yl]-3-oxopropanoate

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Technology Process of ethyl 3-[4-bromo-1-(2,4-dimethylphenyl)-1H-imidazol-5-yl]-3-oxopropanoate

There total 1 articles about ethyl 3-[4-bromo-1-(2,4-dimethylphenyl)-1H-imidazol-5-yl]-3-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 868374-17-8
4-bromo-1-(2,4-dimethylphenyl)-1H-imidazole-5-carbonyl chloride hydrochloride

: 105-53-3
diethyl malonate

: 868374-18-9
ethyl 3-[4-bromo-1-(2,4-dimethylphenyl)-1H-imidazol-5-yl]-3-oxopropanoate

Guidance literature:: diethyl malonate; With methylmagnesium bromide; In tetrahydrofuran; at 0 ℃; for 0.5h;

4-bromo-1-(2,4-dimethylphenyl)-1H-imidazole-5-carbonyl chloride hydrochloride; In tetrahydrofuran; at 20 ℃; for 3h;

Reference yield: 36.0%

: 868374-18-9
ethyl 3-[4-bromo-1-(2,4-dimethylphenyl)-1H-imidazol-5-yl]-3-oxopropanoate

: 16751-59-0
4-heptylamine

: 122-51-0
orthoformic acid triethyl ester

: 868374-19-0
ethyl 2-[4-bromo-1-(2,4-dimethylphenyl)-1H-imidazole-5-carbonyl]-3-(heptan-4-ylamino)acrylate

Guidance literature:: ethyl 3-[4-bromo-1-(2,4-dimethylphenyl)-1H-imidazol-5-yl]-3-oxopropanoate; orthoformic acid triethyl ester; With acetic anhydride; at 120 ℃; for 1.5h;

4-heptylamine; In ethanol; at 0 ℃; for 1h;