9-phenylnaphtho[2,1-e]thiazolo[2,3-c][1,2,4]triazin-4-ium perchlorate

Base Information

Chemical Name:9-phenylnaphtho[2,1-e]thiazolo[2,3-c][1,2,4]triazin-4-ium perchlorate
CAS No.:1638770-51-0
Molecular Formula:C₁₉H₁₂N₃S*ClO₄
Molecular Weight:413.841
Hs Code.:

Synonyms:9-phenylnaphtho[2,1-e]thiazolo[2,3-c][1,2,4]triazin-4-ium perchlorate

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Chemical Property of 9-phenylnaphtho[2,1-e]thiazolo[2,3-c][1,2,4]triazin-4-ium perchlorate

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Technology Process of 9-phenylnaphtho[2,1-e]thiazolo[2,3-c][1,2,4]triazin-4-ium perchlorate

There total 3 articles about 9-phenylnaphtho[2,1-e]thiazolo[2,3-c][1,2,4]triazin-4-ium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 3257-22-5
1-(4-phenylthiazol-2-ylazo)-naphthalen-2-ol

: 1638770-51-0
9-phenylnaphtho[2,1-e]thiazolo[2,3-c][1,2,4]triazin-4-ium perchlorate

Guidance literature:: With perchloric acid; In acetic acid; for 3h; Reflux;
DOI:10.5560/ZNB.2014-4001

Reference yield:

: 135-19-3
β-naphthol

: 1638770-51-0
9-phenylnaphtho[2,1-e]thiazolo[2,3-c][1,2,4]triazin-4-ium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1.1: nitrosylsulfuric acid

1.2: 0 °C / Cooling

2.1: perchloric acid / acetic acid / 3 h / Reflux

With perchloric acid; nitrosylsulfuric acid; In acetic acid;
DOI:10.5560/ZNB.2014-4001

Reference yield:

: 2010-06-2
2-Amino-4-phenylthiazole

: 1638770-51-0
9-phenylnaphtho[2,1-e]thiazolo[2,3-c][1,2,4]triazin-4-ium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1.1: nitrosylsulfuric acid

1.2: 0 °C / Cooling

2.1: perchloric acid / acetic acid / 3 h / Reflux

With perchloric acid; nitrosylsulfuric acid; In acetic acid;
DOI:10.5560/ZNB.2014-4001