1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure

Base Information

Chemical Name:1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure
CAS No.:82417-61-6
Molecular Formula:C₁₆H₁₂N₄O₃
Molecular Weight:308.296
Hs Code.:

Synonyms:1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure

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Chemical Property of 1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure

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Technology Process of 1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure

There total 4 articles about 1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 82417-53-6
1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure-methylester

: 82417-61-6
1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure

Guidance literature:: With sodium hydroxide; In methanol; water; for 1h; Heating;

Reference yield:

: 5281-18-5
benzaldehyde, hydrazone

: 82417-61-6
1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / Et₃N / acetonitrile / 2 h / 50 °C

2: 75 percent / Et₃N / acetonitrile / 1 h / Ambient temperature

3: 93 percent / NaOH / methanol; H₂O / 1 h / Heating

With sodium hydroxide; triethylamine; In methanol; water; acetonitrile;

Reference yield:

: 82418-42-6
Methyl-2-benzylidenhydrazino-2-(phenylhydrazono)acetat

: 82417-61-6
1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Et₃N / acetonitrile / 1 h / Ambient temperature

2: 93 percent / NaOH / methanol; H₂O / 1 h / Heating

With sodium hydroxide; triethylamine; In methanol; water; acetonitrile;