1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure-methylester

Base Information

Chemical Name:1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure-methylester
CAS No.:82417-53-6
Molecular Formula:C₁₇H₁₄N₄O₃
Molecular Weight:322.323
Hs Code.:

Synonyms:1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure-methylester

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Chemical Property of 1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure-methylester

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Technology Process of 1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure-methylester

There total 3 articles about 1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 75-44-5
phosgene

: 82418-42-6
Methyl-2-benzylidenhydrazino-2-(phenylhydrazono)acetat

: 82417-53-6
1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure-methylester

Guidance literature:: With triethylamine; In acetonitrile; for 1h; Ambient temperature;

Reference yield:

: 5281-18-5
benzaldehyde, hydrazone

: 82417-53-6
1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / Et₃N / acetonitrile / 2 h / 50 °C

2: 75 percent / Et₃N / acetonitrile / 1 h / Ambient temperature

With triethylamine; In acetonitrile;

Reference yield:

: 100-52-7
benzaldehyde

: 82417-53-6
1-(Phenyl)-4-benzylidenamino-4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-carbonsaeure-methylester

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / 80percent H₄N₂ solution

2: 86 percent / Et₃N / acetonitrile / 2 h / 50 °C

3: 75 percent / Et₃N / acetonitrile / 1 h / Ambient temperature

With hydrazine hydrate; triethylamine; In acetonitrile;