(R)-[3-(tert-butyloxycarbonyl)]-4-(3-bromo-phenyl)-4-methyl-[1,1,3]oxathiazolidine-2,2-dioxide

Base Information

Chemical Name:(R)-[3-(tert-butyloxycarbonyl)]-4-(3-bromo-phenyl)-4-methyl-[1,1,3]oxathiazolidine-2,2-dioxide
CAS No.:1352419-84-1
Molecular Formula:C₁₄H₁₈BrNO₅S
Molecular Weight:392.271
Hs Code.:

Synonyms:(R)-[3-(tert-butyloxycarbonyl)]-4-(3-bromo-phenyl)-4-methyl-[1,1,3]oxathiazolidine-2,2-dioxide

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Chemical Property of (R)-[3-(tert-butyloxycarbonyl)]-4-(3-bromo-phenyl)-4-methyl-[1,1,3]oxathiazolidine-2,2-dioxide

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Technology Process of (R)-[3-(tert-butyloxycarbonyl)]-4-(3-bromo-phenyl)-4-methyl-[1,1,3]oxathiazolidine-2,2-dioxide

There total 7 articles about (R)-[3-(tert-butyloxycarbonyl)]-4-(3-bromo-phenyl)-4-methyl-[1,1,3]oxathiazolidine-2,2-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1352419-83-0
(R)-[3-(tert-butyloxycarbonyl)-4-(3-bromo-phenyl)]-4-methyl-[1,1,3]oxathiazolidine-2-oxide

: 1352419-84-1
(R)-[3-(tert-butyloxycarbonyl)]-4-(3-bromo-phenyl)-4-methyl-[1,1,3]oxathiazolidine-2,2-dioxide

Guidance literature:: With ruthenium trichloride; sodium periodate; In water; acetonitrile; at 0 - 20 ℃;

Reference yield:

: 953741-63-4
rac-2-amino-2-(3-bromo-phenyl)-propionitrile

: 1352419-84-1
(R)-[3-(tert-butyloxycarbonyl)]-4-(3-bromo-phenyl)-4-methyl-[1,1,3]oxathiazolidine-2,2-dioxide

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride / 96 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -15 - 0 °C

3.1: Chiralpak_.(R). Daicel / carbon dioxide; methanol / Resolution of racemate

4.1: sodium hydrogencarbonate / tetrahydrofuran / 15 h / 0 - 20 °C

5.1: thionyl chloride / acetonitrile / 0.5 h / -40 °C / Inert atmosphere

5.2: -40 - 20 °C

6.1: sodium periodate; ruthenium trichloride / acetonitrile; water / 0 - 20 °C

With hydrogenchloride; ruthenium trichloride; sodium periodate; lithium aluminium tetrahydride; thionyl chloride; sodium hydrogencarbonate; In tetrahydrofuran; methanol; carbon dioxide; water; acetonitrile;

Reference yield:

: 1213181-85-1
(2R)-2-amino-2-(3-bromophenyl)-propan-1-ol

: 1352419-84-1
(R)-[3-(tert-butyloxycarbonyl)]-4-(3-bromo-phenyl)-4-methyl-[1,1,3]oxathiazolidine-2,2-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate / tetrahydrofuran / 15 h / 0 - 20 °C

2.1: thionyl chloride / acetonitrile / 0.5 h / -40 °C / Inert atmosphere

2.2: -40 - 20 °C

3.1: sodium periodate; ruthenium trichloride / acetonitrile; water / 0 - 20 °C

With ruthenium trichloride; sodium periodate; thionyl chloride; sodium hydrogencarbonate; In tetrahydrofuran; water; acetonitrile;