(R)-7-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-5-methylene-heptan-1-ol

Base Information

Chemical Name:(R)-7-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-5-methylene-heptan-1-ol
CAS No.:208658-99-5
Molecular Formula:C₂₁H₃₆O₃Si
Molecular Weight:364.601
Hs Code.:

Synonyms:(R)-7-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-5-methylene-heptan-1-ol

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Chemical Property of (R)-7-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-5-methylene-heptan-1-ol

Chemical Property:

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Technology Process of (R)-7-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-5-methylene-heptan-1-ol

There total 7 articles about (R)-7-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-5-methylene-heptan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 208658-97-3
Benzoic acid (R)-7-benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-5-methylene-heptyl ester

: 208658-99-5
(R)-7-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-5-methylene-heptan-1-ol

Guidance literature:: With lithium methanolate; In methanol;
DOI:10.1016/S0040-4039(98)00682-0

Reference yield:

: 58558-53-5
(((3-methylbut-3-en-1-yl)oxy)methyl)benzene

: 208658-99-5
(R)-7-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-5-methylene-heptan-1-ol

Guidance literature:: Multi-step reaction with 7 steps

1: 49 percent / EtAlCl₂

2: 94 percent / DIBAL-H

3: 88 percent / D-(+)-DET, Ti(O-i-Pr)4, t-BuOOH

4: 93 percent / Red-Al

5: 93 percent

6: 97 percent

7: 93 percent / CH₃OLi / methanol

With titanium(IV) isopropylate; tert.-butylhydroperoxide; D-(+)-DET; lithium methanolate; ethylaluminum dichloride; diisobutylaluminium hydride; sodium bis(2-methoxyethoxy)aluminium dihydride; In methanol;
DOI:10.1016/S0040-4039(98)00682-0

Reference yield:

: 208658-93-9
(R)-7-Benzyloxy-5-methylene-heptane-1,3-diol

: 208658-99-5
(R)-7-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-5-methylene-heptan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent

2: 97 percent

3: 93 percent / CH₃OLi / methanol

With lithium methanolate; In methanol;
DOI:10.1016/S0040-4039(98)00682-0