(3S,4S)-4-(tert-butoxycarbonyl)amino-4-methoxycarbonyl-3-methyl-2-oxoazepane

Base Information

Chemical Name:(3S,4S)-4-(tert-butoxycarbonyl)amino-4-methoxycarbonyl-3-methyl-2-oxoazepane
CAS No.:1252809-31-6
Molecular Formula:C₁₄H₂₄N₂O₅
Molecular Weight:300.355
Hs Code.:

Synonyms:(3S,4S)-4-(tert-butoxycarbonyl)amino-4-methoxycarbonyl-3-methyl-2-oxoazepane

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Chemical Property of (3S,4S)-4-(tert-butoxycarbonyl)amino-4-methoxycarbonyl-3-methyl-2-oxoazepane

Chemical Property:

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Technology Process of (3S,4S)-4-(tert-butoxycarbonyl)amino-4-methoxycarbonyl-3-methyl-2-oxoazepane

There total 1 articles about (3S,4S)-4-(tert-butoxycarbonyl)amino-4-methoxycarbonyl-3-methyl-2-oxoazepane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: C₂₂H₃₀N₂O₇

: 1315455-79-8
(3R,4S)-1-tert-butoxycarbonyl-1,6-diazaspiro[3.5]nonane-2,5-dione

: 1252809-31-6
(3S,4S)-4-(tert-butoxycarbonyl)amino-4-methoxycarbonyl-3-methyl-2-oxoazepane

: 1315455-77-6
(3R,4S)-4-(tert-butoxycarbonyl)amino-4-methoxycarbonyl-3-methyl-2-oxoazepane

Guidance literature:: With palladium 10% on activated carbon; hydrogen; under 760.051 Torr; diastereoselective reaction;
DOI:10.1021/jo200894d

Reference yield: 91.0%

: 1252809-31-6
(3S,4S)-4-(tert-butoxycarbonyl)amino-4-methoxycarbonyl-3-methyl-2-oxoazepane

: 100-39-0
benzyl bromide

: 1252809-39-4
(3S,4S)-1-benzyl-4-(tert-butoxycarbonyl)amino-4-methoxycarbonyl-3-methyl-2-oxoazepane

Guidance literature:: With tert-butylimino-tri(pyrrolidino)phosphorane; In acetonitrile; Microwave irradiation;
DOI:10.1039/c5ob00429b

Reference yield:

: 1252809-31-6
(3S,4S)-4-(tert-butoxycarbonyl)amino-4-methoxycarbonyl-3-methyl-2-oxoazepane

: methyl 3-(tert-butoxycarbonyl)amino-2-methyl-3-(1’-benzyl-2’-oxopiperidin-3’-yl)propionate

Guidance literature:: Multi-step reaction with 3 steps

1: tert-butylimino-tri(pyrrolidino)phosphorane / acetonitrile / Microwave irradiation

2: methanol; sodium hydroxide / 20 °C / Microwave irradiation

3: dichloromethane

With methanol; tert-butylimino-tri(pyrrolidino)phosphorane; sodium hydroxide; In dichloromethane; acetonitrile;
DOI:10.1039/c5ob00429b