4,4-difluoro-8-{3,5-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]phenyl}-1,3,5,7-tetramethyl-2,6-bis{2-[methyl(pyridin-2-ylmethyl)amino]methylpyridin-5-yl}-4-bora-3a,4a-diaza-s-indacene

Base Information

• Chemical Name: 4,4-difluoro-8-{3,5-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]phenyl}-1,3,5,7-tetramethyl-2,6-bis{2-[methyl(pyridin-2-ylmethyl)amino]methylpyridin-5-yl}-4-bora-3a,4a-diaza-s-indacene
• CAS No.: 1151762-02-5
• Molecular Formula: C₅₇H₆₉BF₂N₈O₈
• Molecular Weight: 1043.03

Synonyms:4,4-difluoro-8-{3,5-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]phenyl}-1,3,5,7-tetramethyl-2,6-bis{2-[methyl(pyridin-2-ylmethyl)amino]methylpyridin-5-yl}-4-bora-3a,4a-diaza-s-indacene

Chemical Property of 4,4-difluoro-8-{3,5-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]phenyl}-1,3,5,7-tetramethyl-2,6-bis{2-[methyl(pyridin-2-ylmethyl)amino]methylpyridin-5-yl}-4-bora-3a,4a-diaza-s-indacene

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Technology Process of 4,4-difluoro-8-{3,5-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]phenyl}-1,3,5,7-tetramethyl-2,6-bis{2-[methyl(pyridin-2-ylmethyl)amino]methylpyridin-5-yl}-4-bora-3a,4a-diaza-s-indacene

There total 2 articles about 4,4-difluoro-8-{3,5-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]phenyl}-1,3,5,7-tetramethyl-2,6-bis{2-[methyl(pyridin-2-ylmethyl)amino]methylpyridin-5-yl}-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

4,4-difluoro-2,6-bis[(2-formyl)pyrid-5-yl]-8-{3,5-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]phenyl}1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene (1151762-01-4) + 2-(methylaminomethyl)pyridine hydrobromide (1150632-95-3) → 4,4-difluoro-8-{3,5-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]phenyl}-1,3,5,7-tetramethyl-2,6-bis{2-[methyl(pyridin-2-ylmethyl)amino]methylpyridin-5-yl}-4-bora-3a,4a-diaza-s-indacene (1151762-02-5)

Guidance literature:

With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1021/ja9008369

Reference yield: 64.0%

4,4-difluoro-2,6-bis[(2-formyl)pyrid-5-yl]-8-{3,5-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]phenyl}1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene (1151762-01-4) + N-methyl-2-pyridinemethanamine (21035-59-6) → 4,4-difluoro-8-{3,5-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]phenyl}-1,3,5,7-tetramethyl-2,6-bis{2-[methyl(pyridin-2-ylmethyl)amino]methylpyridin-5-yl}-4-bora-3a,4a-diaza-s-indacene (1151762-02-5)

Guidance literature:

With sodium tris(acetoxy)borohydride; In dichloromethane; acetic acid; room temp.;

DOI:10.1021/ja9008369

Reference yield: 85.0%

zinc(II) nitrate (10196-18-6) + 4,4-difluoro-8-{3,5-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]phenyl}-1,3,5,7-tetramethyl-2,6-bis{2-[methyl(pyridin-2-ylmethyl)amino]methylpyridin-5-yl}-4-bora-3a,4a-diaza-s-indacene (1151762-02-5) → 2Zn(2+)*(HO(CH2CH2O)3)2C6H3C(NC4(CH3)2NC6H5NCH3C6H6N)2BF2*4NO3(1-)=(HO(CH2CH2O)3)2C6H3C(NC4(CH3)2N3C13H14)2BF2Zn2(NO3)4

Guidance literature:

In acetonitrile; room temp.; elem. anal.;

DOI:10.1021/ja9008369

upstream raw materials:

4,4-difluoro-2,6-bis[(2-formyl)pyrid-5-yl]-8-{3,5-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]phenyl}1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

N-methyl-2-pyridinemethanamine

2-(methylaminomethyl)pyridine hydrobromide

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