(Z)-1-ethyl-5-(2-(4-methoxy-2-nitrophenyl)hydrazono)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile

Base Information

• Chemical Name: (Z)-1-ethyl-5-(2-(4-methoxy-2-nitrophenyl)hydrazono)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile
• CAS No.: 1399166-04-1
• Molecular Formula: C₁₆H₁₅N₅O₅
• Molecular Weight: 357.326
• Mol file: 1399166-04-1.mol

Synonyms:(Z)-1-ethyl-5-(2-(4-methoxy-2-nitrophenyl)hydrazono)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile

Chemical Property of (Z)-1-ethyl-5-(2-(4-methoxy-2-nitrophenyl)hydrazono)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z)-1-ethyl-5-(2-(4-methoxy-2-nitrophenyl)hydrazono)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile

There total 1 articles about (Z)-1-ethyl-5-(2-(4-methoxy-2-nitrophenyl)hydrazono)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

3-cyano-1-ethyl-6-hydroxy-4-methyl-2-pyridone (28141-13-1) + 4-methoxy-2-nitroaniline (96-96-8) → (Z)-1-ethyl-5-(2-(4-methoxy-2-nitrophenyl)hydrazono)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile (1399166-04-1)

Guidance literature:

4-methoxy-2-nitroaniline; With hydrogenchloride; sodium nitrite; In water; at -5 ℃; for 0.5h;

3-cyano-1-ethyl-6-hydroxy-4-methyl-2-pyridone; In methanol; water; at 0 - 5 ℃; for 3h;

DOI:10.1039/c2dt31102j

Reference yield: 47.0%

(Z)-1-ethyl-5-(2-(4-methoxy-2-nitrophenyl)hydrazono)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile (1399166-04-1) + copper(II) acetate monohydrate (6046-93-1) → C64H56Cu2N20O20 (1399166-06-3)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 5h;

DOI:10.1039/c2dt31102j

upstream raw materials:

3-cyano-1-ethyl-6-hydroxy-4-methyl-2-pyridone

4-methoxy-2-nitroaniline

Downstream raw materials:

C₆₄H₅₆Cu₂N₂₀O₂₀