1H-Indene-1-carboxylicacid,2,3-dihydro-3-(hydroxyimino)-,methylester,(E)-(9CI)

Base Information

Chemical Name:1H-Indene-1-carboxylicacid,2,3-dihydro-3-(hydroxyimino)-,methylester,(E)-(9CI)
CAS No.:111634-90-3
Molecular Formula:C₁₁H₁₁NO₃
Molecular Weight:205.213
Hs Code.:
Mol file:111634-90-3.mol

Synonyms:1H-Indene-1-carboxylicacid,2,3-dihydro-3-(hydroxyimino)-,methylester,(E)-(9CI)

Suppliers and Price of 1H-Indene-1-carboxylicacid,2,3-dihydro-3-(hydroxyimino)-,methylester,(E)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 1H-Indene-1-carboxylicacid,2,3-dihydro-3-(hydroxyimino)-,methylester,(E)-(9CI)

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of 1H-Indene-1-carboxylicacid,2,3-dihydro-3-(hydroxyimino)-,methylester,(E)-(9CI)

There total 3 articles about 1H-Indene-1-carboxylicacid,2,3-dihydro-3-(hydroxyimino)-,methylester,(E)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 29427-70-1
methyl 3-oxo-2,3-dihydro-1H-indene-1-carboxylate

: 185122-64-9,111634-90-3,111634-92-5
Methyl 3-hydroxyimino-1-indanecarboxylate

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; for 1h; Heating;
DOI:10.1021/jm00397a029

Reference yield:

: 29427-69-8
3-oxoindan-1-carboxylic acid

: 185122-64-9,111634-90-3,111634-92-5
Methyl 3-hydroxyimino-1-indanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 5.75 g / H₂SO₄ / 16 h / Heating

2: 91 percent / H₂NOH*HCl; NaOAc / aq. ethanol / 1 h / Heating

With sulfuric acid; hydroxylamine hydrochloride; sodium acetate; In ethanol;
DOI:10.1055/s-2001-10811

Reference yield:

: 1131-15-3,112489-85-7
2-phenylsuccinic anhydride

: 185122-64-9,111634-90-3,111634-92-5
Methyl 3-hydroxyimino-1-indanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: AlCl₃ / 1,2-dichloro-ethane / 0.67 h / 20 °C

2: 5.75 g / H₂SO₄ / 16 h / Heating

3: 91 percent / H₂NOH*HCl; NaOAc / aq. ethanol / 1 h / Heating

With aluminium trichloride; sulfuric acid; hydroxylamine hydrochloride; sodium acetate; In ethanol; 1,2-dichloro-ethane;
DOI:10.1055/s-2001-10811