C₄₇H₇₃N₅O₁₃

Base Information

Chemical Name:C₄₇H₇₃N₅O₁₃
CAS No.:185461-52-3
Molecular Formula:C₄₇H₇₃N₅O₁₃
Molecular Weight:916.122
Hs Code.:

C<sub>47</sub>H<sub>73</sub>N<sub>5</sub>O<sub>13</sub>

Synonyms:C₄₇H₇₃N₅O₁₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₇H₇₃N₅O₁₃

Chemical Property:

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Technology Process of C₄₇H₇₃N₅O₁₃

There total 14 articles about C₄₇H₇₃N₅O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 185461-57-8
C₄₇H₇₅N₅O₁₄

: 185461-52-3
C₄₇H₇₃N₅O₁₃

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-<(dimethylamino)-1H-1,2,3-triazolo<4,5-b>pyridin-1-ylmethylene>-N-methylmethanaminium hexafluorophosphate N-oxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 17h; Ambient temperature;
DOI:10.1021/jo961932h

Reference yield:

: 15260-10-3
N-Boc-O-benzyl-L-threonine

: 185461-52-3
C₄₇H₇₃N₅O₁₃

Guidance literature:: Multi-step reaction with 7 steps

1: 78 percent Turnov_. / Li₂CO₃, 4 Angstroem molecular sieves / dimethylformamide / 18 h / Ambient temperature

2: 97 percent / H₂ / Pd/C / methanol / 1 h / 760 Torr / Ambient temperature

3: 88 percent / DCC, DMAP / CH₂Cl₂ / 15 h / Ambient temperature

4: 72 percent / aq. HF / acetonitrile / 7 h / -25 - -15 °C

5: 1-hydroxybenzotriazole, N-<(1H-benzotriazol-1-yl)(dimethylamino)methylene>-N-methylmethanaminium hexafluorophosphate N-oxide, N,N-diisopropylethylamine / tetrahydrofuran / 4 h / -10 - -5 °C

6: 99 percent / H₂ / Pd/C / tetrahydrofuran / 3 h / 760 Torr / Ambient temperature

7: 76 percent / N-<(dimethylamino)-1H-1,2,3-triazolo<4,5-b>pyridin-1-ylmethylene>-N-methylmethanaminium hexafluorophosphate N-oxide, 1-hydroxy-7-azabenzotriazole, N,N-diisopropylethylamine / tetrahydrofuran / 17 h / Ambient temperature

With dmap; 1-hydroxy-7-aza-benzotriazole; 4 A molecular sieve; N-<(1H-benzotriazol-1-yl)(dimethylamino)methylene>-N-methylmethanaminium hexafluorophosphate N-oxide; N-<(dimethylamino)-1H-1,2,3-triazolo<4,5-b>pyridin-1-ylmethylene>-N-methylmethanaminium hexafluorophosphate N-oxide; hydrogen fluoride; hydrogen; lithium carbonate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo961932h

Reference yield:

: 126587-71-1
Boc-threonine [(2-trimethylsilyl)ethoxy]methyl ester

: 185461-52-3
C₄₇H₇₃N₅O₁₃

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / DCC, DMAP / CH₂Cl₂ / 15 h / Ambient temperature

2: 72 percent / aq. HF / acetonitrile / 7 h / -25 - -15 °C

3: 1-hydroxybenzotriazole, N-<(1H-benzotriazol-1-yl)(dimethylamino)methylene>-N-methylmethanaminium hexafluorophosphate N-oxide, N,N-diisopropylethylamine / tetrahydrofuran / 4 h / -10 - -5 °C

4: 99 percent / H₂ / Pd/C / tetrahydrofuran / 3 h / 760 Torr / Ambient temperature

5: 76 percent / N-<(dimethylamino)-1H-1,2,3-triazolo<4,5-b>pyridin-1-ylmethylene>-N-methylmethanaminium hexafluorophosphate N-oxide, 1-hydroxy-7-azabenzotriazole, N,N-diisopropylethylamine / tetrahydrofuran / 17 h / Ambient temperature

With dmap; 1-hydroxy-7-aza-benzotriazole; N-<(1H-benzotriazol-1-yl)(dimethylamino)methylene>-N-methylmethanaminium hexafluorophosphate N-oxide; N-<(dimethylamino)-1H-1,2,3-triazolo<4,5-b>pyridin-1-ylmethylene>-N-methylmethanaminium hexafluorophosphate N-oxide; hydrogen fluoride; hydrogen; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jo961932h