Technology Process of 2-[2]naphthyl-cyclohex-2-enone
There total 4 articles about 2-[2]naphthyl-cyclohex-2-enone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; sodium carbonate;
In
1,2-dimethoxyethane; water;
at 25 - 30 ℃;
for 15h;
DOI:10.1021/acs.orglett.1c01689
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate; iodine; dmap / tetrahydrofuran; water / 3 h / 20 °C
2: potassium carbonate / aq. buffer / 6 h / 70 °C / pH 7.5 / Ionic liquid
With
dmap; iodine; potassium carbonate;
In
tetrahydrofuran; water;
2: |Suzuki-Miyaura Coupling;
DOI:10.1039/d1gc00372k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diethyl ether
2: propionic acid; aqueous HCl / Erwaermen des Reaktionsprodukts mit aethanol. KOH und Erhitzen des danach erhaltenen Reaktionsprodukts mit wss. HCl, wss. Formaldehyd und Dioxan
With
hydrogenchloride; diethyl ether; propionic acid;
DOI:10.1039/jr9570001293
