3-bromo-N-cyclopropyl-5-[(1E)-3-methoxyprop-1-en-1-yl]-4-methylbenzamide

Base Information

Chemical Name:3-bromo-N-cyclopropyl-5-[(1E)-3-methoxyprop-1-en-1-yl]-4-methylbenzamide
CAS No.:1229245-22-0
Molecular Formula:C₁₅H₁₈BrNO₂
Molecular Weight:324.217
Hs Code.:

Synonyms:3-bromo-N-cyclopropyl-5-[(1E)-3-methoxyprop-1-en-1-yl]-4-methylbenzamide

Suppliers and Price of 3-bromo-N-cyclopropyl-5-[(1E)-3-methoxyprop-1-en-1-yl]-4-methylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3-bromo-N-cyclopropyl-5-[(1E)-3-methoxyprop-1-en-1-yl]-4-methylbenzamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of 3-bromo-N-cyclopropyl-5-[(1E)-3-methoxyprop-1-en-1-yl]-4-methylbenzamide

There total 2 articles about 3-bromo-N-cyclopropyl-5-[(1E)-3-methoxyprop-1-en-1-yl]-4-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1229245-24-2
3,5-dibromo-N-cyclopropyl-4-methylbenzamide

: 165059-42-7,934342-48-0
(E)-3-methoxy-1-propenylboronic acid pinacol ester

: 1229245-22-0
3-bromo-N-cyclopropyl-5-[(1E)-3-methoxyprop-1-en-1-yl]-4-methylbenzamide

Guidance literature:: With sodium carbonate; trans-dichlorobis(triphenylphosphine)palladium(II); In water; N,N-dimethyl-formamide; at 100 ℃; for 1h; Inert atmosphere of nitrogen;

Reference yield:

: 67973-32-4
3,5-dibromo-4-methylbenzoic acid

: 1229245-22-0
3-bromo-N-cyclopropyl-5-[(1E)-3-methoxyprop-1-en-1-yl]-4-methylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 18 h / 20 °C

2: sodium carbonate / trans-dichlorobis(triphenylphosphine)palladium(II) / water; N,N-dimethyl-formamide / 1 h / 100 °C / Inert atmosphere of nitrogen

With sodium carbonate; N-ethyl-N,N-diisopropylamine; HATU; trans-dichlorobis(triphenylphosphine)palladium(II); In water; N,N-dimethyl-formamide; 2: Suzuki Coupling;