Z-Ser-Leu-Gly-OMe

Base Information

Chemical Name:Z-Ser-Leu-Gly-OMe
CAS No.:107540-38-5
Molecular Formula:C₃₂H₃₈N₃O₁₀P
Molecular Weight:655.642
Hs Code.:

Synonyms:Z-Ser-Leu-Gly-OMe

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Chemical Property of Z-Ser-Leu-Gly-OMe

Chemical Property:

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Technology Process of Z-Ser-Leu-Gly-OMe

There total 3 articles about Z-Ser-Leu-Gly-OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 107540-26-1
Z-Ser-Leu-Gly-OMe

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 107540-38-5
Z-Ser-Leu-Gly-OMe

Guidance literature:: With pyridine; 1.) -10 deg C, 2.5 h, 2.) 4 deg C, 18 h;
DOI:10.1021/jo00385a023

Reference yield:

: 5084-98-0,62188-57-2,109453-36-3
methyl N-benzyloxycarbonyl-L-leucylglicynate

: 107540-38-5
Z-Ser-Leu-Gly-OMe

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / H₂, 2N HCl / Pd/C / methanol; ethanol / 18 h / 1551.4 Torr

2: 66 percent / 1-hydroxybenzotriazole (HOBt), N-methylmorpholine, dicyclohexylcarbodiimide (DCC) / dimethylformamide / 1.) -10 deg C, 1 h, 2.) room temp., 18 h

3: 94 percent / pyridine / 1.) -10 deg C, 2.5 h, 2.) 4 deg C, 18 h

With 4-methyl-morpholine; pyridine; hydrogenchloride; hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00385a023

Reference yield:

: 39622-13-4,120746-40-9,120746-41-0
(S)-methyl 2-(2-amino-4-methylpentanamido)acetate hydrochloride

: 107540-38-5
Z-Ser-Leu-Gly-OMe

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / 1-hydroxybenzotriazole (HOBt), N-methylmorpholine, dicyclohexylcarbodiimide (DCC) / dimethylformamide / 1.) -10 deg C, 1 h, 2.) room temp., 18 h

2: 94 percent / pyridine / 1.) -10 deg C, 2.5 h, 2.) 4 deg C, 18 h

With 4-methyl-morpholine; pyridine; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1021/jo00385a023