(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 2-hydroxycyclohex-1-enecarboxylate

Base Information

Chemical Name:(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 2-hydroxycyclohex-1-enecarboxylate
CAS No.:1452877-22-3
Molecular Formula:C₁₅H₂₄O₅
Molecular Weight:284.353
Hs Code.:

Synonyms:(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 2-hydroxycyclohex-1-enecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 2-hydroxycyclohex-1-enecarboxylate

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Technology Process of (2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 2-hydroxycyclohex-1-enecarboxylate

There total 1 articles about (2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 2-hydroxycyclohex-1-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 3663-46-5
5-hydroxymethyl-2,2,5-trimethyl-1,3-dioxane

: 4840-68-0
2-hydroxy-1-cyclohexenecarboxylic acid ethyl ester

: 1452877-22-3
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 2-hydroxycyclohex-1-enecarboxylate

Guidance literature:: With Otera’s Catalyst; In toluene; for 72h; Molecular sieve; Reflux;
DOI:10.1039/c3ob40800k

Reference yield: 26.0%

: 75-11-6
diiodomethane

: 1452877-22-3
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 2-hydroxycyclohex-1-enecarboxylate

: 1452877-23-4
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 1-(iodomethyl)-2-oxocyclohexanecarboxylate

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; mineral oil; at 20 ℃; for 20h;
DOI:10.1039/c3ob40800k

Reference yield:

: 1452877-22-3
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 2-hydroxycyclohex-1-enecarboxylate

: 1452877-27-8
C₄₈H₇₂O₁₈

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / mineral oil; dimethyl sulfoxide / 20 h / 20 °C

2: potassium carbonate / 72 h / 70 °C / Inert atmosphere

3: methanol / 6 h / 20 °C

With methanol; sodium hydride; potassium carbonate; In dimethyl sulfoxide; mineral oil; 2: |Grob-Eschenmoser Fragmentation;
DOI:10.1039/c3ob40800k