(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 1-(iodomethyl)-2-oxocyclohexanecarboxylate

Base Information

Chemical Name:(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 1-(iodomethyl)-2-oxocyclohexanecarboxylate
CAS No.:1452877-23-4
Molecular Formula:C₁₆H₂₅IO₅
Molecular Weight:424.276
Hs Code.:

Synonyms:(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 1-(iodomethyl)-2-oxocyclohexanecarboxylate

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Chemical Property of (2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 1-(iodomethyl)-2-oxocyclohexanecarboxylate

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Technology Process of (2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 1-(iodomethyl)-2-oxocyclohexanecarboxylate

There total 3 articles about (2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 1-(iodomethyl)-2-oxocyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 75-11-6
diiodomethane

: 1452877-22-3
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 2-hydroxycyclohex-1-enecarboxylate

: 1452877-23-4
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 1-(iodomethyl)-2-oxocyclohexanecarboxylate

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; mineral oil; at 20 ℃; for 20h;
DOI:10.1039/c3ob40800k

Reference yield:

: 4840-68-0
2-hydroxy-1-cyclohexenecarboxylic acid ethyl ester

: 1452877-23-4
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 1-(iodomethyl)-2-oxocyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: Otera’s Catalyst / toluene / 72 h / Molecular sieve; Reflux

2: sodium hydride / mineral oil; dimethyl sulfoxide / 20 h / 20 °C

With Otera’s Catalyst; sodium hydride; In dimethyl sulfoxide; toluene; mineral oil;
DOI:10.1039/c3ob40800k

Reference yield:

: 3663-46-5
5-hydroxymethyl-2,2,5-trimethyl-1,3-dioxane

: 1452877-23-4
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 1-(iodomethyl)-2-oxocyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: Otera’s Catalyst / toluene / 72 h / Molecular sieve; Reflux

2: sodium hydride / mineral oil; dimethyl sulfoxide / 20 h / 20 °C

With Otera’s Catalyst; sodium hydride; In dimethyl sulfoxide; toluene; mineral oil;
DOI:10.1039/c3ob40800k