N-(benzyloxycarbonyl)-N'-1H,1H,2H,2H-perfluorodecylcarbamoyloxymethylbis(hydroxymethyl)aminomethane

Base Information

Chemical Name:N-(benzyloxycarbonyl)-N'-1H,1H,2H,2H-perfluorodecylcarbamoyloxymethylbis(hydroxymethyl)aminomethane
CAS No.:420107-86-4
Molecular Formula:C₂₃H₂₁F₁₇N₂O₆
Molecular Weight:744.402
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)-N'-1H,1H,2H,2H-perfluorodecylcarbamoyloxymethylbis(hydroxymethyl)aminomethane

Suppliers and Price of N-(benzyloxycarbonyl)-N'-1H,1H,2H,2H-perfluorodecylcarbamoyloxymethylbis(hydroxymethyl)aminomethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(benzyloxycarbonyl)-N'-1H,1H,2H,2H-perfluorodecylcarbamoyloxymethylbis(hydroxymethyl)aminomethane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N-(benzyloxycarbonyl)-N'-1H,1H,2H,2H-perfluorodecylcarbamoyloxymethylbis(hydroxymethyl)aminomethane

There total 6 articles about N-(benzyloxycarbonyl)-N'-1H,1H,2H,2H-perfluorodecylcarbamoyloxymethylbis(hydroxymethyl)aminomethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 420107-83-1
5-N-(benzyloxycarbonyl)amino-5-N'-1H,1H,2H,2H-perfluorodecylcarbamoyloxymethyl-2,2-dimethyl-1,3-dioxane

: 420107-86-4
N-(benzyloxycarbonyl)-N'-1H,1H,2H,2H-perfluorodecylcarbamoyloxymethylbis(hydroxymethyl)aminomethane

Guidance literature:: With Montmorillonite K₁₀; In dichloromethane;
DOI:10.1039/b104958p

Reference yield:

: 89373-67-1
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecanoylchloride

: 420107-86-4
N-(benzyloxycarbonyl)-N'-1H,1H,2H,2H-perfluorodecylcarbamoyloxymethylbis(hydroxymethyl)aminomethane

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaN₃ / acetone; H₂O / 10 - 15 °C

1.2: 62 percent / cyclohexane

2.1: 92 percent / diazabicyclooctane / toluene / 6 h / pH 8 - 9 / Heating

3.1: 90 percent / montmorillonite K₁₀ / CH₂Cl₂

With 1,4-diaza-bicyclo[2.2.2]octane; sodium azide; Montmorillonite K₁₀; In dichloromethane; water; acetone; toluene; 1.2: Curtius Rearrangement;
DOI:10.1039/b104958p

Reference yield:

: 142010-50-2
3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl isocyanate

: 420107-86-4
N-(benzyloxycarbonyl)-N'-1H,1H,2H,2H-perfluorodecylcarbamoyloxymethylbis(hydroxymethyl)aminomethane

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / diazabicyclooctane / toluene / 6 h / pH 8 - 9 / Heating

2: 90 percent / montmorillonite K₁₀ / CH₂Cl₂

With 1,4-diaza-bicyclo[2.2.2]octane; Montmorillonite K₁₀; In dichloromethane; toluene;
DOI:10.1039/b104958p