<1-Methyl-2,4-dioxo-3-(triphenylphosphoranyliden)cyclobutyl>triphenylphosphonium-iodid

Base Information

Chemical Name:<1-Methyl-2,4-dioxo-3-(triphenylphosphoranyliden)cyclobutyl>triphenylphosphonium-iodid
CAS No.:20369-59-9
Molecular Formula:C₄₁H₃₃O₂P₂*I
Molecular Weight:746.564
Hs Code.:

Synonyms:<1-Methyl-2,4-dioxo-3-(triphenylphosphoranyliden)cyclobutyl>triphenylphosphonium-iodid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <1-Methyl-2,4-dioxo-3-(triphenylphosphoranyliden)cyclobutyl>triphenylphosphonium-iodid

Chemical Property:

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Technology Process of <1-Methyl-2,4-dioxo-3-(triphenylphosphoranyliden)cyclobutyl>triphenylphosphonium-iodid

There total 3 articles about <1-Methyl-2,4-dioxo-3-(triphenylphosphoranyliden)cyclobutyl>triphenylphosphonium-iodid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 73818-55-0,15596-07-3
Bestmann ylide

: 74-88-4
methyl iodide

: 20369-59-9
<1-Methyl-2,4-dioxo-3-(triphenylphosphoranyliden)cyclobutyl>triphenylphosphonium-iodid

Guidance literature:: In benzene; for 48h; Ambient temperature;

Reference yield:

: 7533-53-1
O₂CC(PPh₃)2

: 20369-59-9
<1-Methyl-2,4-dioxo-3-(triphenylphosphoranyliden)cyclobutyl>triphenylphosphonium-iodid

Guidance literature:: Multi-step reaction with 2 steps

1: bis-(2-methoxy-ethyl) ether

2: Ph₃PO / CH₂Cl₂

With Triphenylphosphine oxide; In dichloromethane; diethylene glycol dimethyl ether;
DOI:10.1021/ja01016a045

Reference yield:

: 103559-83-7
hexaphenylcarbodiphosphorane

: 20369-59-9
<1-Methyl-2,4-dioxo-3-(triphenylphosphoranyliden)cyclobutyl>triphenylphosphonium-iodid

Guidance literature:: Multi-step reaction with 3 steps

2: bis-(2-methoxy-ethyl) ether

3: Ph₃PO / CH₂Cl₂

With Triphenylphosphine oxide; In dichloromethane; diethylene glycol dimethyl ether;
DOI:10.1021/ja01016a045