Technology Process of C47H50N8O11S
There total 21 articles about C47H50N8O11S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium phosphate;
In
dichloromethane; water;
at 22 ℃;
DOI:10.1021/jm400560z
- Guidance literature:
-
Multi-step reaction with 8 steps
1: sodium hydroxide / methanol; water / 0.17 h / Reflux
2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C
3: potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C
4: triethylamine / dichloromethane / 1 h / 0 °C
5: potassium iodide / N,N-dimethyl-formamide / 20 °C
6: hydrazine hydrate / ethanol / 1 h / Reflux
7: ethyl acetate / 2 h / 50 °C
8: potassium phosphate / dichloromethane; water / 22 °C
With
potassium phosphate; hydroxylamine hydrochloride; sodium acetate; potassium carbonate; hydrazine hydrate; triethylamine; potassium iodide; sodium hydroxide;
In
methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm400560z
- Guidance literature:
-
Multi-step reaction with 8 steps
1: sodium hydroxide / methanol; water / 0.17 h / Reflux
2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C
3: potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C
4: triethylamine / dichloromethane / 1 h / 0 °C
5: potassium iodide / N,N-dimethyl-formamide / 20 °C
6: hydrazine hydrate / ethanol / 1 h / Reflux
7: ethyl acetate / 2 h / 50 °C
8: potassium phosphate / dichloromethane; water / 22 °C
With
potassium phosphate; hydroxylamine hydrochloride; sodium acetate; potassium carbonate; hydrazine hydrate; triethylamine; potassium iodide; sodium hydroxide;
In
methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm400560z