4,4'-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N-hexyldiphenylamine

Base Information

Chemical Name:4,4'-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N-hexyldiphenylamine
CAS No.:865163-50-4
Molecular Formula:C₃₀H₄₅B₂NO₄
Molecular Weight:505.314
Hs Code.:

Synonyms:4,4'-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N-hexyldiphenylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N-hexyldiphenylamine

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Technology Process of 4,4'-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N-hexyldiphenylamine

There total 5 articles about 4,4'-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N-hexyldiphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: N-hexyl-4,4'-dibromodiphenylamine

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 865163-50-4
4,4'-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N-hexyldiphenylamine

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃;
DOI:10.1021/ma051102i

Reference yield: 24.0%

: N-hexyl-4,4'-dibromodiphenylamine

: 73183-34-3
bis(pinacol)diborane

: 865163-50-4
4,4'-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N-hexyldiphenylamine

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium acetate; In toluene; at 110 ℃; for 18h; Inert atmosphere;
DOI:10.1039/c2nj40963a

Reference yield:

: 16292-17-4
bis(4-bromophenyl)amine

: 865163-50-4
4,4'-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N-hexyldiphenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / t-BuOK / tetrahydrofuran / 24 h / 60 °C

2: 58 percent / n-BuLi / tetrahydrofuran; hexane / 20 °C

With n-butyllithium; potassium tert-butylate; In tetrahydrofuran; hexane;
DOI:10.1021/ma051102i