ethyl 2-{4-[(4-{[(2Z)-2-(4-cyanophenyl)-2-(methoxyimino)ethyl]oxy}benzyl)oxy]phenyl}cyclopropanecarboxylate

Base Information

Chemical Name:ethyl 2-{4-[(4-{[(2Z)-2-(4-cyanophenyl)-2-(methoxyimino)ethyl]oxy}benzyl)oxy]phenyl}cyclopropanecarboxylate
CAS No.:1356600-32-2
Molecular Formula:C₂₉H₂₈N₂O₅
Molecular Weight:484.552
Hs Code.:

Synonyms:ethyl 2-{4-[(4-{[(2Z)-2-(4-cyanophenyl)-2-(methoxyimino)ethyl]oxy}benzyl)oxy]phenyl}cyclopropanecarboxylate

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Chemical Property of ethyl 2-{4-[(4-{[(2Z)-2-(4-cyanophenyl)-2-(methoxyimino)ethyl]oxy}benzyl)oxy]phenyl}cyclopropanecarboxylate

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Technology Process of ethyl 2-{4-[(4-{[(2Z)-2-(4-cyanophenyl)-2-(methoxyimino)ethyl]oxy}benzyl)oxy]phenyl}cyclopropanecarboxylate

There total 3 articles about ethyl 2-{4-[(4-{[(2Z)-2-(4-cyanophenyl)-2-(methoxyimino)ethyl]oxy}benzyl)oxy]phenyl}cyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98017-60-8
2-(4-methoxyphenyl)cyclopropanecarboxylic acid ethyl ester

: 1356600-32-2
ethyl 2-{4-[(4-{[(2Z)-2-(4-cyanophenyl)-2-(methoxyimino)ethyl]oxy}benzyl)oxy]phenyl}cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron tribromide / dichloromethane / 0.5 h / 0 °C

1.2: 0 °C

2.1: potassium carbonate / acetonitrile / 15 h / 0 - 70 °C

With boron tribromide; potassium carbonate; In dichloromethane; acetonitrile;

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1356600-32-2
ethyl 2-{4-[(4-{[(2Z)-2-(4-cyanophenyl)-2-(methoxyimino)ethyl]oxy}benzyl)oxy]phenyl}cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

1.2: 1 h / 0 °C / Inert atmosphere

2.1: potassium hydroxide / dimethyl sulfoxide / 0.17 h / 0 - 20 °C

2.2: 3 h / 20 °C

3.1: boron tribromide / dichloromethane / 0.5 h / 0 °C

3.2: 0 °C

4.1: potassium carbonate / acetonitrile / 15 h / 0 - 70 °C

With boron tribromide; sodium hydride; potassium carbonate; potassium hydroxide; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 51507-22-3
(Z)-ethyl 3-(4-methoxyphenyl)acrylate

: 1356600-32-2
ethyl 2-{4-[(4-{[(2Z)-2-(4-cyanophenyl)-2-(methoxyimino)ethyl]oxy}benzyl)oxy]phenyl}cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 0.17 h / 0 - 20 °C

1.2: 3 h / 20 °C

2.1: boron tribromide / dichloromethane / 0.5 h / 0 °C

2.2: 0 °C

3.1: potassium carbonate / acetonitrile / 15 h / 0 - 70 °C

With boron tribromide; potassium carbonate; potassium hydroxide; In dichloromethane; dimethyl sulfoxide; acetonitrile;