([1-(3,5-dinitrophenyl)-4-methyl-3-nitropyrazol-5-yl]sulfanyl)acetanilide

Base Information

Chemical Name:([1-(3,5-dinitrophenyl)-4-methyl-3-nitropyrazol-5-yl]sulfanyl)acetanilide
CAS No.:1246855-89-9
Molecular Formula:C₁₈H₁₄N₆O₇S
Molecular Weight:458.411
Hs Code.:

Synonyms:([1-(3,5-dinitrophenyl)-4-methyl-3-nitropyrazol-5-yl]sulfanyl)acetanilide

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Chemical Property of ([1-(3,5-dinitrophenyl)-4-methyl-3-nitropyrazol-5-yl]sulfanyl)acetanilide

Chemical Property:

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Technology Process of ([1-(3,5-dinitrophenyl)-4-methyl-3-nitropyrazol-5-yl]sulfanyl)acetanilide

There total 3 articles about ([1-(3,5-dinitrophenyl)-4-methyl-3-nitropyrazol-5-yl]sulfanyl)acetanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1246855-82-2
1-(3,5-dinitrophenyl)-4-methyl-3,5-dinitropyrazole

: 4822-44-0
2-mercapto-N-phenylacetamide

: 1246855-89-9
([1-(3,5-dinitrophenyl)-4-methyl-3-nitropyrazol-5-yl]sulfanyl)acetanilide

Guidance literature:: With potassium carbonate; In acetonitrile; at 25 ℃; for 20h;
DOI:10.1007/s11172-009-0290-1

Reference yield:

: 99-35-4
1,3,5-trinitrobenzene

: 1246855-89-9
([1-(3,5-dinitrophenyl)-4-methyl-3-nitropyrazol-5-yl]sulfanyl)acetanilide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 4 h / Reflux

2: sulfuric acid; nitric acid / 2 h / 100 - 105 °C

3: potassium carbonate / acetonitrile / 20 h / 25 °C

With sulfuric acid; nitric acid; potassium carbonate; In acetonitrile;
DOI:10.1007/s11172-009-0290-1

Reference yield:

: 1246855-83-3
1-(3,5-dinitrophenyl)-4-methyl-3-nitropyrazole

: 1246855-89-9
([1-(3,5-dinitrophenyl)-4-methyl-3-nitropyrazol-5-yl]sulfanyl)acetanilide

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; nitric acid / 2 h / 100 - 105 °C

2: potassium carbonate / acetonitrile / 20 h / 25 °C

With sulfuric acid; nitric acid; potassium carbonate; In acetonitrile;
DOI:10.1007/s11172-009-0290-1