3-methyl-2,6,8-trinitropyrazolo[1,5-a][3,1]benzothiazine-5-carboxanilide

Base Information

Chemical Name:3-methyl-2,6,8-trinitropyrazolo[1,5-a][3,1]benzothiazine-5-carboxanilide
CAS No.:1246855-91-3
Molecular Formula:C₁₈H₁₂N₆O₇S
Molecular Weight:456.395
Hs Code.:

Synonyms:3-methyl-2,6,8-trinitropyrazolo[1,5-a][3,1]benzothiazine-5-carboxanilide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methyl-2,6,8-trinitropyrazolo[1,5-a][3,1]benzothiazine-5-carboxanilide

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Technology Process of 3-methyl-2,6,8-trinitropyrazolo[1,5-a][3,1]benzothiazine-5-carboxanilide

There total 4 articles about 3-methyl-2,6,8-trinitropyrazolo[1,5-a][3,1]benzothiazine-5-carboxanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1246855-89-9
([1-(3,5-dinitrophenyl)-4-methyl-3-nitropyrazol-5-yl]sulfanyl)acetanilide

: 1246855-91-3
3-methyl-2,6,8-trinitropyrazolo[1,5-a][3,1]benzothiazine-5-carboxanilide

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 48h;
DOI:10.1007/s11172-009-0290-1

Reference yield:

: 99-35-4
1,3,5-trinitrobenzene

: 1246855-91-3
3-methyl-2,6,8-trinitropyrazolo[1,5-a][3,1]benzothiazine-5-carboxanilide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile / 4 h / Reflux

2: sulfuric acid; nitric acid / 2 h / 100 - 105 °C

3: potassium carbonate / acetonitrile / 20 h / 25 °C

4: potassium carbonate / acetonitrile / 48 h / 20 °C

With sulfuric acid; nitric acid; potassium carbonate; In acetonitrile;
DOI:10.1007/s11172-009-0290-1

Reference yield:

: 1246855-83-3
1-(3,5-dinitrophenyl)-4-methyl-3-nitropyrazole

: 1246855-91-3
3-methyl-2,6,8-trinitropyrazolo[1,5-a][3,1]benzothiazine-5-carboxanilide

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; nitric acid / 2 h / 100 - 105 °C

2: potassium carbonate / acetonitrile / 20 h / 25 °C

3: potassium carbonate / acetonitrile / 48 h / 20 °C

With sulfuric acid; nitric acid; potassium carbonate; In acetonitrile;
DOI:10.1007/s11172-009-0290-1