<1-Methyl-3-(1,2,3,4-tetrahydro-4-methyl-3-phenyl-1-(phenylseleno)cyclopentindol-2-yl)-1H-indol-2-yl>phenylmethanone

Base Information

• Chemical Name: <1-Methyl-3-(1,2,3,4-tetrahydro-4-methyl-3-phenyl-1-(phenylseleno)cyclopentindol-2-yl)-1H-indol-2-yl>phenylmethanone
• CAS No.: 127229-95-2
• Molecular Formula: C₄₀H₃₂N₂OSe
• Molecular Weight: 635.667

Synonyms:<1-Methyl-3-(1,2,3,4-tetrahydro-4-methyl-3-phenyl-1-(phenylseleno)cyclopentindol-2-yl)-1H-indol-2-yl>phenylmethanone

Chemical Property of <1-Methyl-3-(1,2,3,4-tetrahydro-4-methyl-3-phenyl-1-(phenylseleno)cyclopentindol-2-yl)-1H-indol-2-yl>phenylmethanone

Chemical Property:

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Technology Process of <1-Methyl-3-(1,2,3,4-tetrahydro-4-methyl-3-phenyl-1-(phenylseleno)cyclopentindol-2-yl)-1H-indol-2-yl>phenylmethanone

There total 10 articles about <1-Methyl-3-(1,2,3,4-tetrahydro-4-methyl-3-phenyl-1-(phenylseleno)cyclopentindol-2-yl)-1H-indol-2-yl>phenylmethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

C34H26N2O (127229-93-0) + Benzeneselenol (645-96-5) → <1-Methyl-3-(1,2,3,4-tetrahydro-4-methyl-3-phenyl-1-(phenylseleno)cyclopentindol-2-yl)-1H-indol-2-yl>phenylmethanone (127229-95-2)

Guidance literature:

With zinc(II) iodide; In dichloromethane; for 1h; Ambient temperature;

DOI:10.1021/jo00299a031

Reference yield:

cis-bicyclo[3. 3. 0]octane-3,7-dione (51716-63-3) → <1-Methyl-3-(1,2,3,4-tetrahydro-4-methyl-3-phenyl-1-(phenylseleno)cyclopentindol-2-yl)-1H-indol-2-yl>phenylmethanone (127229-95-2)

Guidance literature:

Multi-step reaction with 5 steps

1: 50 percent

2: 56 percent / SeO₂ / dioxane / 48 h / Heating

3: 96 percent / tetrahydrofuran / -78 to 25 deg C

4: 83 percent / p-TsOH, molecular sieves / benzene / 0.08 h / Ambient temperature

5: ZnI₂

With selenium(IV) oxide; molecular sieve; toluene-4-sulfonic acid; zinc(II) iodide; In tetrahydrofuran; 1,4-dioxane; benzene;

DOI:10.1016/S0040-4020(01)80896-6

Reference yield:

phenylhydrazine (100-63-0) → <1-Methyl-3-(1,2,3,4-tetrahydro-4-methyl-3-phenyl-1-(phenylseleno)cyclopentindol-2-yl)-1H-indol-2-yl>phenylmethanone (127229-95-2)

Guidance literature:

Multi-step reaction with 6 steps

1: 20 percent / HCl / ethanol / Δ

2: 90 percent / NaH / tetrahydrofuran

3: 56 percent / SeO₂ / dioxane / 48 h / Heating

4: 96 percent / tetrahydrofuran / -78 to 25 deg C

5: 83 percent / p-TsOH, molecular sieves / benzene / 0.08 h / Ambient temperature

6: ZnI₂

With selenium(IV) oxide; molecular sieve; sodium hydride; toluene-4-sulfonic acid; zinc(II) iodide; hydrogenchloride; In tetrahydrofuran; 1,4-dioxane; ethanol; benzene;

DOI:10.1016/S0040-4020(01)80896-6

upstream raw materials:

C₃₄H₂₆N₂O

Benzeneselenol

C₃₄H₂₆N₂O

cis-bicyclo[3. 3. 0]octane-3,7-dione

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