C₄₆H₆₂N₈O₁₀S

Base Information

Chemical Name:C₄₆H₆₂N₈O₁₀S
CAS No.:1292220-45-1
Molecular Formula:C₄₆H₆₂N₈O₁₀S
Molecular Weight:919.112
Hs Code.:

C<sub>46</sub>H<sub>62</sub>N<sub>8</sub>O<sub>10</sub>S

Synonyms:C₄₆H₆₂N₈O₁₀S

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Chemical Property of C₄₆H₆₂N₈O₁₀S

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Technology Process of C₄₆H₆₂N₈O₁₀S

There total 9 articles about C₄₆H₆₂N₈O₁₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1292220-43-9
C₂₂H₂₉N₃O₅S

: 1292220-39-3
C₃₁H₃₈IN₅O₆

: 1292220-45-1
C₄₆H₆₂N₈O₁₀S

Guidance literature:: C₂₂H₂₉N₃O₅S; C₃₁H₃₈IN₅O₆; With triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 22 - 85 ℃; for 14.25h; Inert atmosphere; Sealed vessel;

With methanol; In N,N-dimethyl-formamide; at 90 ℃; for 3h; Sealed vessel;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1292220-45-1
C₄₆H₆₂N₈O₁₀S

Guidance literature:: Multi-step reaction with 4 steps

1.1: ethanol / 2 h / 20 °C / Inert atmosphere

1.2: 3.33 h / 0 - 20 °C

1.3: 23 h / 20 °C

2.1: N,N,N,N,-tetramethylethylenediamine; copper(II) acetate monohydrate / water; methanol / 5.5 h / 20 °C

3.1: pyridine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

4.1: triethylamine / tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / N,N-dimethyl-formamide / 14.25 h / 22 - 85 °C / Inert atmosphere; Sealed vessel

4.2: 3 h / 90 °C / Sealed vessel

With pyridine; triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N,N,N,-tetramethylethylenediamine; copper(II) acetate monohydrate; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 618-58-6
3,5-dibromobenzoic acid

: 1292220-45-1
C₄₆H₆₂N₈O₁₀S

Guidance literature:: Multi-step reaction with 4 steps

1.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.08 h / 22 °C / Inert atmosphere

1.2: 24 h / 22 °C

2.1: potassium carbonate / L-proline; copper(l) iodide / dimethyl sulfoxide / 20 h / 85 °C / Inert atmosphere

3.1: triethylamine / tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / dimethyl sulfoxide; tetrahydrofuran / 3 h / 45 - 50 °C / Inert atmosphere; Sealed vessel

3.2: 0.5 h / 45 °C / Inert atmosphere

4.1: triethylamine / tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / N,N-dimethyl-formamide / 14.25 h / 22 - 85 °C / Inert atmosphere; Sealed vessel

4.2: 3 h / 90 °C / Sealed vessel

With potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; L-proline; In tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide;