3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-α/β-D-galactopyranosyl N-phenyltrifluoroacetimidate

Base Information

Chemical Name:3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-α/β-D-galactopyranosyl N-phenyltrifluoroacetimidate
CAS No.:1448429-95-5
Molecular Formula:C₃₇H₃₄Cl₃F₃N₂O₆
Molecular Weight:766.041
Hs Code.:

Synonyms:3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-α/β-D-galactopyranosyl N-phenyltrifluoroacetimidate

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Chemical Property of 3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-α/β-D-galactopyranosyl N-phenyltrifluoroacetimidate

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Technology Process of 3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-α/β-D-galactopyranosyl N-phenyltrifluoroacetimidate

There total 2 articles about 3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-α/β-D-galactopyranosyl N-phenyltrifluoroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 61881-19-4
2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

: N-((3R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-hydroxy-tetrahydro-pyran-3-yl)-2,2,2-trichloro-acetamide

: 1448429-95-5
3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-α/β-D-galactopyranosyl N-phenyltrifluoroacetimidate

Guidance literature:: With caesium carbonate; In acetone; at 20 ℃; for 4h;

Reference yield: 5.0%

: 61881-19-4
2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

: N-((3R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-hydroxy-tetrahydro-pyran-3-yl)-2,2,2-trichloro-acetamide

: 1448429-95-5
3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-α/β-D-galactopyranosyl N-phenyltrifluoroacetimidate

: 1448429-96-6
2-trichloromethyl-(3,4,6-tri-O-benzyl-1,2-dideoxy-α-D-galactopyrano)-[2,1-d]-2-oxazoline

Guidance literature:: With caesium carbonate; In acetone; at 20 ℃; for 4h;
DOI:10.1002/ejoc.201300180

Reference yield: 63.0%

: 1448429-95-5
3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-α/β-D-galactopyranosyl N-phenyltrifluoroacetimidate

: 1448429-83-1
benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

: 1448430-02-1
benzyl (3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranosyl)-(1→2)-(4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

: 1448430-03-2
benzyl (3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranosyl)-(1→2)-(4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

Guidance literature:: 3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-α/β-D-galactopyranosyl N-phenyltrifluoroacetimidate; benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate; In dichloromethane; at 20 ℃; for 1h; Microwave irradiation;

With trimethylsilyl trifluoromethanesulfonate; triethylamine; In N,N-dimethyl-formamide; at -78 ℃; for 0.333333h;
DOI:10.1002/ejoc.201300180