Technology Process of C13H15NO4
There total 1 articles about C13H15NO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran;
at 0 ℃;
for 1h;
- Guidance literature:
-
C13H15NO4;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 0 ℃;
for 0.5h;
With
sodium hydroxide;
In
tetrahydrofuran; water;
for 0.25h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C
1.2: 0.25 h
2.1: Dess-Martin periodane / dichloromethane / 0.08 h / 22 °C / Reflux
3.1: sodium cyanoborohydride / methanol / 1 h / 0 °C
3.2: 4 h
4.1: hydrogenchloride / 1,4-dioxane; diethyl ether / 22 °C
5.1: diethylamine / trisodium tris(3-sulfophenyl)phosphine; palladium diacetate / acetonitrile; water / 0.25 h / 22 °C
With
hydrogenchloride; lithium aluminium tetrahydride; sodium cyanoborohydride; Dess-Martin periodane; diethylamine;
trisodium tris(3-sulfophenyl)phosphine; palladium diacetate;
In
tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; dichloromethane; water; acetonitrile;