2-methoxy-1-[4-(oxiranylmethoxy)phenyl]ethanone

Base Information

Chemical Name:2-methoxy-1-[4-(oxiranylmethoxy)phenyl]ethanone
CAS No.:110458-44-1
Molecular Formula:C12H14 O4
Molecular Weight:222.241
Hs Code.:2914509090
Mol file:110458-44-1.mol

Synonyms:Ethanone,2-methoxy-1-[4-(oxiranylmethoxy)phenyl]- (9CI); Ethanone,2-methoxy-1-[4-(oxiranylmethoxy)phenyl]-, (?à)-

Suppliers and Price of 2-methoxy-1-[4-(oxiranylmethoxy)phenyl]ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Methoxy-1-[4-(oxiranylmethoxy)phenyl]ethanone
50mg
$ 110.00

Medical Isotopes, Inc.
2-methoxy-1-[4-(oxiranylmethoxy)phenyl]ethanone
50 mg
$ 860.00

American Custom Chemicals Corporation
2-METHOXY-1-(4-(OXIRANYLMETHOXY)PHENYL)ETHANONE 95.00%
5MG
$ 504.32

Total 2 raw suppliers

Chemical Property of 2-methoxy-1-[4-(oxiranylmethoxy)phenyl]ethanone

Chemical Property:

Boiling Point:367.2±22.0 °C(Predicted)
PSA：48.06000
Density:1.181±0.06 g/cm3(Predicted)
LogP:1.29330
Storage Temp.:Refrigerator
Solubility.:Chloroform (Slightly), Methanol (Slightly)

Purity/Quality:

97% ^*data from raw suppliers

2-Methoxy-1-[4-(oxiranylmethoxy)phenyl]ethanone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 2-Methoxy-1-[4-(oxiranylmethoxy)phenyl]ethanone (cas# 110458-44-1) is a compound useful in organic synthesis.

Technology Process of 2-methoxy-1-[4-(oxiranylmethoxy)phenyl]ethanone

There total 4 articles about 2-methoxy-1-[4-(oxiranylmethoxy)phenyl]ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2491-38-5
2-bromo-1-(4'-hydroxyphenyl)-1-ethanone

: 110458-44-1
2-Methoxy-1-(4-oxiranylmethoxy-phenyl)-ethanone

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / methanol / 0.5 h / Heating

2: 80 percent / NaOH / dimethylformamide / 2 h / Heating

3: 67 percent / aq. HCl / acetone / 2 h / Heating

4: 1.) TsCl, 2.) NaH / 1.) pyridine, 0 deg C, 4 d, 2.) reflux, 90 min

With hydrogenchloride; sodium hydroxide; sodium hydride; p-toluenesulfonyl chloride; In methanol; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00396a009

Reference yield:

: 32136-81-5
alpha-methoxy-4-hydroxyacetophenone

: 110458-44-1
2-Methoxy-1-(4-oxiranylmethoxy-phenyl)-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / NaOH / dimethylformamide / 2 h / Heating

2: 67 percent / aq. HCl / acetone / 2 h / Heating

3: 1.) TsCl, 2.) NaH / 1.) pyridine, 0 deg C, 4 d, 2.) reflux, 90 min

With hydrogenchloride; sodium hydroxide; sodium hydride; p-toluenesulfonyl chloride; In N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00396a009

Reference yield:

: 110458-42-9
1-[4-(2,2-Dimethyl-[1,3]dioxolan-4-ylmethoxy)-phenyl]-2-methoxy-ethanone

: 110458-44-1
2-Methoxy-1-(4-oxiranylmethoxy-phenyl)-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / aq. HCl / acetone / 2 h / Heating

2: 1.) TsCl, 2.) NaH / 1.) pyridine, 0 deg C, 4 d, 2.) reflux, 90 min

With hydrogenchloride; sodium hydride; p-toluenesulfonyl chloride; In acetone;
DOI:10.1021/jm00396a009