C₂₅H₂₄N₂O₈

Base Information

Chemical Name:C₂₅H₂₄N₂O₈
CAS No.:213480-36-5
Molecular Formula:C₂₅H₂₄N₂O₈
Molecular Weight:480.474
Hs Code.:

C<sub>25</sub>H<sub>24</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:C₂₅H₂₄N₂O₈

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Chemical Property of C₂₅H₂₄N₂O₈

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Technology Process of C₂₅H₂₄N₂O₈

There total 5 articles about C₂₅H₂₄N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 213480-35-4
C₂₅H₂₈N₂O₆

: 213480-36-5
C₂₅H₂₄N₂O₈

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; potassium bromide; In phosphate buffer; dichloromethane; at -5 - 0 ℃; pH=7;
DOI:10.1021/jo980354x

Reference yield:

: 59779-75-8
diethyl (4R,5R)-2,2-dimethyl-1,3-dioxolane-4,5-dicarboxylate

: 213480-36-5
C₂₅H₂₄N₂O₈

Guidance literature:: Multi-step reaction with 5 steps

1: DIBAL / toluene; hexane / 3 h / -78 °C

2: toluene; hexane / 14 h / -78 - 20 °C

3: triethylamine / CH₂Cl₂ / 14 h / -20 - 20 °C

4: 1.80 g / hydrogen / Pd/C / ethanol / 15 h / 20 °C / 760 Torr

5: 98 percent / sodium hypochlorite; 2,2,6,6-tetramethylpiperidin-1-oxyl; potassium bromide / CH₂Cl₂; aq. phosphate buffer / -5 - 0 °C / pH 7

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; hydrogen; diisobutylaluminium hydride; triethylamine; potassium bromide; palladium on activated charcoal; In phosphate buffer; ethanol; hexane; dichloromethane; toluene; 1: Reduction / 2: Condensation / 3: Cycloaddition / 4: Hydrogenolysis / 5: Oxidation;
DOI:10.1021/jo980354x

Reference yield:

: 122137-20-6
(4R,5R)-2,2-Dimethyl-[1,3]dioxolane-4,5-dicarbaldehyde

: 213480-36-5
C₂₅H₂₄N₂O₈

Guidance literature:: Multi-step reaction with 4 steps

1: toluene; hexane / 14 h / -78 - 20 °C

2: triethylamine / CH₂Cl₂ / 14 h / -20 - 20 °C

3: 1.80 g / hydrogen / Pd/C / ethanol / 15 h / 20 °C / 760 Torr

4: 98 percent / sodium hypochlorite; 2,2,6,6-tetramethylpiperidin-1-oxyl; potassium bromide / CH₂Cl₂; aq. phosphate buffer / -5 - 0 °C / pH 7

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; hydrogen; triethylamine; potassium bromide; palladium on activated charcoal; In phosphate buffer; ethanol; hexane; dichloromethane; toluene; 1: Condensation / 2: Cycloaddition / 3: Hydrogenolysis / 4: Oxidation;
DOI:10.1021/jo980354x